lithium 1,3-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-1,3,2-diazaborol-2-ide

Base Information

• Chemical Name: lithium 1,3-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-1,3,2-diazaborol-2-ide
• CAS No.: 948054-44-2
• Molecular Formula: C₂₆H₃₆BLiN₂
• Molecular Weight: 394.337
• Mol file: 948054-44-2.mol

Synonyms:lithium 1,3-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-1,3,2-diazaborol-2-ide

Chemical Property of lithium 1,3-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-1,3,2-diazaborol-2-ide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of lithium 1,3-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-1,3,2-diazaborol-2-ide

There total 3 articles about lithium 1,3-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-1,3,2-diazaborol-2-ide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N'-bis(2,6-diisopropylphenyl)-2-bromo-2,3-dihydro-1H-1,3,2-diazaborole (915703-81-0) → lithium 1,3-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-1,3,2-diazaborol-2-ide (948054-44-2)

Guidance literature:

With naphthalene; lithium; In tetrahydrofuran; at -45 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ja8057919

Reference yield:

C2H2N2BI(2,6-(iPr)2C6H3)2 (1082608-12-5) → lithium 1,3-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-1,3,2-diazaborol-2-ide (948054-44-2)

Guidance literature:

With naphthalene; lithium; In tetrahydrofuran; at -45 ℃; for 6h; Inert atmosphere;

DOI:10.1021/ja8057919

Reference yield:

N,N'-bis(2,6-diisopropylphenyl)-2-chloro-1,3,2-diazaborole (1008748-17-1) → lithium 1,3-bis(2,6-diisopropylphenyl)-2,3-dihydro-1H-1,3,2-diazaborol-2-ide (948054-44-2)

Guidance literature:

With 4,4'-di-tert-butylbiphenyl; lithium; In tetrahydrofuran; at -45 ℃; for 10h; Inert atmosphere;

DOI:10.1021/ja8057919

upstream raw materials:

N,N'-bis(2,6-diisopropylphenyl)-2-bromo-2,3-dihydro-1H-1,3,2-diazaborole

N,N'-bis(2,6-diisopropylphenyl)-2-chloro-1,3,2-diazaborole

C₂H₂N₂BI(2,6-(iPr)2C₆H₃)2

Downstream raw materials:

[(CH)₂(N(2,6-iPr₂C₆H₃))₂]BH

(C₂H₂N₂(2,6-(iPr)2C₆H₃)2)BCOOPh

N,N'-bis(2,6-diisopropylphenyl)-2-bromo-2,3-dihydro-1H-1,3,2-diazaborole

(C₂H₂N₂(2,6-(iPr)2C₆H₃)2)BPh