Ethyl 2-(diethylcarbamoyl)benzoate

Base Information

Chemical Name:Ethyl 2-(diethylcarbamoyl)benzoate
CAS No.:24677-02-9
Molecular Formula:C14H19 N O3
Molecular Weight:249.31
Hs Code.:2924299090
DSSTox Substance ID:DTXSID90500221
Nikkaji Number:J3.086.117E
Wikidata:Q82351650
Mol file:24677-02-9.mol

Synonyms:24677-02-9;ETHYL 2-(DIETHYLCARBAMOYL)BENZOATE;Benzoic acid, 2-[(diethylamino)carbonyl]-, ethyl ester;N,N-DIETHYL-PHTHALAMIC ACID ETHYL ESTER;DTXSID90500221;AKOS015967686

Suppliers and Price of Ethyl 2-(diethylcarbamoyl)benzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N,N-DIETHYL-PHTHALAMIC ACID ETHYL ESTER 95.00%
5MG
$ 498.87

Total 7 raw suppliers

Chemical Property of Ethyl 2-(diethylcarbamoyl)benzoate

Chemical Property:

Vapor Pressure:2.19E-06mmHg at 25°C
Refractive Index:1.517
Boiling Point:393°C at 760 mmHg
PKA:-1.65±0.70(Predicted)
Flash Point:191.5°C
PSA：46.61000
Density:1.073g/cm³
LogP:2.34530
XLogP3:2.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:249.13649347
Heavy Atom Count:18
Complexity:287

Purity/Quality:

95% ^*data from raw suppliers

N,N-DIETHYL-PHTHALAMIC ACID ETHYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C(=O)C1=CC=CC=C1C(=O)OCC

Technology Process of Ethyl 2-(diethylcarbamoyl)benzoate

There total 5 articles about Ethyl 2-(diethylcarbamoyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 88-10-8
N,N-diethylcarbamyl chloride

: (2-(ethoxycarbonyl)phenyl)zinc(II) bromide

: 24677-02-9
ethyl 2-(N,N-diethylaminocarbonyl)benzoate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; for 24h; Reflux;
DOI:10.1016/j.tetlet.2012.04.114

Reference yield: 51.0%

: 88-10-8
N,N-diethylcarbamyl chloride

: 346656-34-6
2-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzoic acid ethyl ester

: 24677-02-9
ethyl 2-(N,N-diethylaminocarbonyl)benzoate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; cesium fluoride; In tetrahydrofuran; at 80 ℃; for 16h;
DOI:10.1021/jo050459h