1,2-Ethane-1,2-d2-diol, 1,2-diphenyl-

Base Information

Chemical Name:1,2-Ethane-1,2-d2-diol, 1,2-diphenyl-
CAS No.:36239-19-7
Molecular Formula:C₁₄H₁₄O₂
Molecular Weight:216.248
Hs Code.:
DSSTox Substance ID:DTXSID001285996

Synonyms:1,2-Ethane-1,2-d2-diol, 1,2-diphenyl-;36239-19-7;DTXSID001285996;1,2-Dideuterio-1,2-diphenylethane-1,2-diol

Suppliers and Price of 1,2-Ethane-1,2-d2-diol, 1,2-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1,2-Ethane-1,2-d2-diol, 1,2-diphenyl-

Chemical Property:

XLogP3:1.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:216.111933177
Heavy Atom Count:16
Complexity:171

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(C(C2=CC=CC=C2)O)O
Isomeric SMILES:[2H]C(C1=CC=CC=C1)(C([2H])(C2=CC=CC=C2)O)O

Technology Process of 1,2-Ethane-1,2-d2-diol, 1,2-diphenyl-

There total 7 articles about 1,2-Ethane-1,2-d2-diol, 1,2-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 134-81-6
benzil

: 36239-19-7
<1,2-2H2>-1,2-diphenyl-1,2-ethanediol

Guidance literature:: With sodium borodeuteride; In methanol; for 1h; Ambient temperature;
DOI:10.1002/jlcr.2580360109

Reference yield: 80.0%

: 5284-44-6
trans-1,2-dideuteriostilbene

: 36239-19-7
<1,2-2H2>-1,2-diphenyl-1,2-ethanediol

Guidance literature:: With N-Bromosuccinimide; potassium carbonate;
DOI:10.1021/acs.orglett.1c02600

Reference yield:

: 645-49-8
cis-stilben

: 36239-19-7
<1,2-2H2>-1,2-diphenyl-1,2-ethanediol

Guidance literature:: Multi-step reaction with 2 steps

1: potassium ethyl xanthogenate; water-d2 / N,N-dimethyl-formamide / 24 h / 150 °C / Schlenk technique

2: N-Bromosuccinimide; potassium carbonate

With N-Bromosuccinimide; water-d2; potassium ethyl xanthogenate; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/acs.orglett.1c02600