(S)-methyl 2-(2-chlorophenyl)-2-(2-acetyl-salicylic acyloxy-4,5,6,7-tetrahydro-thieno[3,2-C]pyridine)-5-acetate hydrochloride salt

Base Information

Chemical Name:(S)-methyl 2-(2-chlorophenyl)-2-(2-acetyl-salicylic acyloxy-4,5,6,7-tetrahydro-thieno[3,2-C]pyridine)-5-acetate hydrochloride salt
CAS No.:1403246-13-8
Molecular Formula:C₂₅H₂₂ClNO₆S*ClH
Molecular Weight:536.433
Hs Code.:

Synonyms:(S)-methyl 2-(2-chlorophenyl)-2-(2-acetyl-salicylic acyloxy-4,5,6,7-tetrahydro-thieno[3,2-C]pyridine)-5-acetate hydrochloride salt

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Chemical Property of (S)-methyl 2-(2-chlorophenyl)-2-(2-acetyl-salicylic acyloxy-4,5,6,7-tetrahydro-thieno[3,2-C]pyridine)-5-acetate hydrochloride salt

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Technology Process of (S)-methyl 2-(2-chlorophenyl)-2-(2-acetyl-salicylic acyloxy-4,5,6,7-tetrahydro-thieno[3,2-C]pyridine)-5-acetate hydrochloride salt

There total 4 articles about (S)-methyl 2-(2-chlorophenyl)-2-(2-acetyl-salicylic acyloxy-4,5,6,7-tetrahydro-thieno[3,2-C]pyridine)-5-acetate hydrochloride salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.8%

: 1312440-98-4
(S)-methyl 2-(2-chlorophenyl)-2-(2-acetyl-salicylic acyloxy-4,5,6,7-tetrahydro-thieno[3,2-C]pyridine)-5-acetate

: 1403246-13-8
(S)-methyl 2-(2-chlorophenyl)-2-(2-acetyl-salicylic acyloxy-4,5,6,7-tetrahydro-thieno[3,2-C]pyridine)-5-acetate hydrochloride salt

Guidance literature:: With hydrogenchloride; In diethyl ether; pH=5;

Reference yield:

: 1441-87-8
salicyloyl chloride

: 1403246-13-8
(S)-methyl 2-(2-chlorophenyl)-2-(2-acetyl-salicylic acyloxy-4,5,6,7-tetrahydro-thieno[3,2-C]pyridine)-5-acetate hydrochloride salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.5 h

1.2: 2 h

2.1: hydrogenchloride / diethyl ether / pH 5

With hydrogenchloride; sodium hydride; In diethyl ether; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 527687-26-9
S(+)-2-(2-chlorophenyl)-2-(4,5,6,7-tetrahydro-thieno[3,2-c]pyridine-2(4H)-one)-5-acetic acid methyl ester

: 1403246-13-8
(S)-methyl 2-(2-chlorophenyl)-2-(2-acetyl-salicylic acyloxy-4,5,6,7-tetrahydro-thieno[3,2-C]pyridine)-5-acetate hydrochloride salt

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / mineral oil; N,N-dimethyl-formamide / 0.5 h

1.2: 2 h

2.1: hydrogenchloride / diethyl ether / pH 5

With hydrogenchloride; sodium hydride; In diethyl ether; N,N-dimethyl-formamide; mineral oil;