3-(4-Benzyloxy-butyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester

Base Information

• Chemical Name: 3-(4-Benzyloxy-butyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester
• CAS No.: 179998-87-9
• Molecular Formula: C₂₃H₃₂O₅
• Molecular Weight: 388.504

Synonyms:3-(4-Benzyloxy-butyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester

Chemical Property of 3-(4-Benzyloxy-butyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(4-Benzyloxy-butyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester

There total 4 articles about 3-(4-Benzyloxy-butyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-((Z)-4-Benzyloxy-but-2-enyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester (179998-86-8) → 3-(4-Benzyloxy-butyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester (179998-87-9)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethyl acetate; for 7h; Ambient temperature;

DOI:10.1039/p19960001517

Reference yield:

ethyl 1-methyl-2,4-dioxocyclohexane-1-carboxylate (24730-94-7) → 3-(4-Benzyloxy-butyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester (179998-87-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 30 percent / N-benzyltrimethylammonium hydroxide / methanol; H₂O / 36 h / Ambient temperature

2: 96 percent / pyridinium toluene-p-sulfonate / benzene / 12 h / Heating

3: 99 percent / H₂ / PtO₂ / ethyl acetate / 7 h / Ambient temperature

With hydrogen; pyridinium p-toluenesulfonate; N-benzyl-trimethylammonium hydroxide; platinum(IV) oxide; In methanol; water; ethyl acetate; benzene;

DOI:10.1039/p19960001517

Reference yield:

(Z)-(((4-bromobut-2-en-1-yl)oxy)methyl)benzene (89358-30-5,105875-09-0,88088-58-8) → 3-(4-Benzyloxy-butyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester (179998-87-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 30 percent / N-benzyltrimethylammonium hydroxide / methanol; H₂O / 36 h / Ambient temperature

2: 96 percent / pyridinium toluene-p-sulfonate / benzene / 12 h / Heating

3: 99 percent / H₂ / PtO₂ / ethyl acetate / 7 h / Ambient temperature

With hydrogen; pyridinium p-toluenesulfonate; N-benzyl-trimethylammonium hydroxide; platinum(IV) oxide; In methanol; water; ethyl acetate; benzene;

DOI:10.1039/p19960001517

upstream raw materials:

3-((Z)-4-Benzyloxy-but-2-enyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester

ethyl 1-methyl-2,4-dioxocyclohexane-1-carboxylate

(Z)-(((4-bromobut-2-en-1-yl)oxy)methyl)benzene

Downstream raw materials:

2-(4-benzyloxybutyl)-4-(2-cyanoacetoxy)methyl-4-methylcyclohex-2-en-1-one

2-(4-benzyloxybutyl)-4-hydroxymethyl-4-methylcyclohex-2-en-1-one

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 179998-87-9 3-(4-Benzyloxy-butyl)-4-ethoxy-1-methyl-2-oxo-cyclohex-3-enecarboxylic acid ethyl ester

Send

Send

Metric Ton KG G Pound L ML

Send

Send