(4-NITRO)PHENYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE

Base Information

Chemical Name:(4-NITRO)PHENYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE
CAS No.:24624-78-0
Molecular Formula:C₁₇H₁₉NO₁₀
Molecular Weight:397.339
Hs Code.:
Mol file:24624-78-0.mol

Synonyms:Xylopyranoside,p-nitrophenyl, 2',3',4'-triacetate, b-D- (8CI); Xylopyranoside, p-nitrophenyl, triacetate (7CI)

Suppliers and Price of (4-NITRO)PHENYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(4-NITRO)PHENYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE 95.00%
5MG
$ 504.93

Total 6 raw suppliers

Chemical Property of (4-NITRO)PHENYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE

Chemical Property:

Melting Point:138-140 °C
Boiling Point:501.6±50.0 °C(Predicted)
PSA：143.18000
Density:1.38±0.1 g/cm3(Predicted)
LogP:1.64820

Purity/Quality:

97% ^*data from raw suppliers

(4-NITRO)PHENYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses p-Nitrophenyl β-D-Xylopyranoside Triacetate is an intermediate in the synthesis of p-Nitrophenyl β-D-Xylopyranoside (N509050), a useful compound in organic synthesis.

Technology Process of (4-NITRO)PHENYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE

There total 7 articles about (4-NITRO)PHENYL-2,3,4-TRI-O-ACETYL-BETA-D-XYLOPYRANOSIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 3068-31-3
1-bromo-2,3,4-tri-O-acetyl-α-D-xylopyranose

: 24624-78-0,58902-46-8,67006-13-7,94921-62-7,94921-63-8,109526-97-8
1-O-(4-nitrophenyl)-2,3,4-tri-O-acetyl-β-D-xylopyranoside

Guidance literature:: With potassium carbonate; In acetone; Ambient temperature;
DOI:10.1016/0008-6215(95)00214-E

Reference yield: 45.0%

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 4049-33-6
tetra-O-acetyl-β-D-xylopyranose

: 24624-78-0,58902-46-8,67006-13-7,94921-62-7,94921-63-8,109526-97-8
1-O-(4-nitrophenyl)-2,3,4-tri-O-acetyl-β-D-xylopyranoside

Guidance literature:: tetra-O-acetyl-β-D-xylopyranose; In dichloromethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;

4-nitro-phenol; With boron trifluoride diethyl etherate; In dichloromethane; at 0 ℃; for 4h; Inert atmosphere; Molecular sieve;

Reference yield: 36.0%

: 3945-26-4,4536-02-1,4556-49-4,4556-50-7,16051-71-1,22893-62-5,90822-01-8,108393-17-5
α-D-xylopyranosyl fluoride

: 108-24-7
acetic anhydride

: 2001-96-9
p-nitrophenyl β-D-xylopyranoside

: 4-nitrophenyl (2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-(1->3)-O-2,4-di-O-acetyl-β-D-xylopyranoside

: 162088-89-3
4-nitrophenyl tri-O-acetyl-β-D-xylopyranosyl-(1->4)-2,3-di-O-acetyl-β-D-xyloside

: 4-nitrophenyl O-(2,3,4-tri-O-acetyl-β-D-xylopyranosyl)-(1<*>4)-O-(2,3-di-O-acetyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-acetyl-β-D-xylopyranoside

: 24624-78-0,58902-46-8,67006-13-7,94921-62-7,94921-63-8,109526-97-8
1-O-(4-nitrophenyl)-2,3,4-tri-O-acetyl-β-D-xylopyranoside

Guidance literature:: α-D-xylopyranosyl fluoride; p-nitrophenyl β-D-xylopyranoside; With Bhxglycosynthase E₃₃₄G mutant; at 20 ℃; for 24h; pH=7; aq. phosphate buffer; Enzymatic reaction;

acetic anhydride; With pyridine; dmap; at 20 ℃; for 16h;
DOI:10.1002/cbic.201100229