5,10,15-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>-20-<2-hydroxy-6-(3,3-dimethylbutyryloxy)phenyl>porphine

Base Information

• Chemical Name: 5,10,15-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>-20-<2-hydroxy-6-(3,3-dimethylbutyryloxy)phenyl>porphine
• CAS No.: 151418-41-6
• Molecular Formula: C₈₆H₁₀₀N₄O₁₅
• Molecular Weight: 1429.76

Synonyms:5,10,15-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>-20-<2-hydroxy-6-(3,3-dimethylbutyryloxy)phenyl>porphine

Chemical Property of 5,10,15-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>-20-<2-hydroxy-6-(3,3-dimethylbutyryloxy)phenyl>porphine

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Technology Process of 5,10,15-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>-20-<2-hydroxy-6-(3,3-dimethylbutyryloxy)phenyl>porphine

There total 1 articles about 5,10,15-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>-20-<2-hydroxy-6-(3,3-dimethylbutyryloxy)phenyl>porphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.3%

3,3-dimethylbutanoic acid chloride (7065-46-5) + 5,10,15,20-tetrakis(2,6-bis(hydroxy)phenyl)porphyrin (124901-08-2) → 5,10,15-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>-20-<2-hydroxy-6-(3,3-dimethylbutyryloxy)phenyl>porphine (151418-41-6)

Guidance literature:

With dmap; In tetrahydrofuran; for 4h; Ambient temperature;

DOI:10.1246/bcsj.66.1640

Reference yield: 54.0%

N-acetyl-D,L-valine (96-81-1,3067-19-4,7295-89-8,17916-88-0,67079-28-1,98392-56-4) + 5,10,15-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>-20-<2-hydroxy-6-(3,3-dimethylbutyryloxy)phenyl>porphine (151418-41-6) → 5,10,15-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>-20-<2-<(N-acetylvalyloxy)>-6-(3,3-dimethylbutyryloxy)phenyl>porphine

Guidance literature:

With 4-pyrrolidin-1-ylpyridine; dicyclohexyl-carbodiimide; In tetrahydrofuran; for 10h; Ambient temperature;

DOI:10.1246/bcsj.66.1640

Reference yield: 54.0%

5-(N-imidazolyl)valeric acid chloride (66188-80-5) + 5,10,15-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>-20-<2-hydroxy-6-(3,3-dimethylbutyryloxy)phenyl>porphine (151418-41-6) → 5-<2-(3,3-Dimethylbutyryloxy)-6-(5-imidazolylvaleryloxy)phenyl>-10,15,20-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>porphyrin (142576-58-7)

Guidance literature:

With dmap; In acetonitrile;

DOI:10.1246/cl.1992.799

upstream raw materials:

3,3-dimethylbutanoic acid chloride

5,10,15,20-tetrakis(2,6-bis(hydroxy)phenyl)porphyrin

Downstream raw materials:

5-<2-(3,3-Dimethylbutyryloxy)-6-(5-imidazolylvaleryloxy)phenyl>-10,15,20-tris<2,6-bis(3,3-dimethylbutyryloxy)phenyl>porphyrin

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