Technology Process of (1S,4R,8S)-3-oxo-p-menthan-9-oic acid methyl ester
There total 11 articles about (1S,4R,8S)-3-oxo-p-menthan-9-oic acid methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dihydrogen peroxide; sodium hydroxide / water / 4 h / 30 °C
2: boron trifluoride diethyl etherate / diethyl ether / 20 °C
3: palladium on activated charcoal; hydrogen / ethyl acetate / 1 h / 20 °C / 760.05 Torr
4: sodium periodate; rhodium(III) chloride hydrate; water / tetrachloromethane; acetonitrile / 20 °C
5: diethyl ether / 1 h / 0 °C
With
sodium periodate; rhodium(III) chloride hydrate; palladium on activated charcoal; boron trifluoride diethyl etherate; water; hydrogen; dihydrogen peroxide; sodium hydroxide;
In
tetrachloromethane; diethyl ether; water; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetasy.2011.07.014
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide / methanol / 20 °C
2: boron trifluoride diethyl etherate / diethyl ether / 20 °C
3: palladium on activated charcoal; hydrogen / ethyl acetate / 1 h / 20 °C / 760.05 Torr
4: sodium periodate; rhodium(III) chloride hydrate; water / tetrachloromethane; acetonitrile / 20 °C
5: diethyl ether / 1 h / 0 °C
With
sodium periodate; rhodium(III) chloride hydrate; palladium on activated charcoal; boron trifluoride diethyl etherate; water; hydrogen; sodium hydroxide;
In
methanol; tetrachloromethane; diethyl ether; ethyl acetate; acetonitrile;
DOI:10.1016/j.tetasy.2011.07.014
