1-phenylsulfanyl-2-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

Base Information

• Chemical Name: 1-phenylsulfanyl-2-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline
• CAS No.: 864953-83-3
• Molecular Formula: C₂₄H₂₂N₂O₂S₂
• Molecular Weight: 434.583

Synonyms:1-phenylsulfanyl-2-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

Chemical Property of 1-phenylsulfanyl-2-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

Chemical Property:

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Technology Process of 1-phenylsulfanyl-2-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline

There total 1 articles about 1-phenylsulfanyl-2-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

tris(phenylthio)methane (4832-52-4) + N-tosyl tryptamine (86658-78-8) → 1-phenylsulfanyl-2-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline (864953-83-3)

Guidance literature:

With tin(IV) chloride; In dichloromethane; at -78 - 20 ℃; for 6h;

DOI:10.1021/ol051342i

Reference yield: 98.0%

1-phenylsulfanyl-2-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline (864953-83-3) + ethylmagnesium bromide (925-90-6) → 1‐ethyl‐2‐tosyl‐2,3,4,9‐tetrahydro‐1H‐pyrido[3,4‐b]indole

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 0.2h;

DOI:10.1021/ol051342i

Reference yield: 98.0%

1-phenylsulfanyl-2-(toluene-4-sulfonyl)-2,3,4,9-tetrahydro-1H-β-carboline (864953-83-3) + phenylmagnesium bromide → 2,3,4,9-tetrahydro-1-phenyl-2-tosyl-1H-pyrido[3,4-b]indole (17071-83-9)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 0.2h;

DOI:10.1021/ol051342i

upstream raw materials:

tris(phenylthio)methane

N-tosyl tryptamine

Downstream raw materials:

2,3,4,9-tetrahydro-1-phenyl-2-tosyl-1H-pyrido[3,4-b]indole

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