ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate

Base Information

Chemical Name:ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate
CAS No.:1539220-43-3
Molecular Formula:C₂₄H₃₁NO₄
Molecular Weight:397.514
Hs Code.:

Synonyms:ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate

Chemical Property:

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Technology Process of ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate

There total 1 articles about ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: ethyl 3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylprop-1-en-1-yl)-4-hydroxybenzoate

: 1539220-43-3
ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In 2-methyltetrahydrofuran; water; at 55 ℃; for 21h; under 375.038 Torr; Inert atmosphere;

Reference yield: 76.0%

: 1539220-43-3
ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate

: 250214-40-5
(R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-hydroxymethylphenol hydrochloride

Guidance literature:: ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate; In toluene; at 5 - 20 ℃;

With hydrogenchloride; In water; acetonitrile;

Reference yield:

: 1539220-43-3
ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate

: 286930-02-7,250214-44-9
fesoterodine

Guidance literature:: Multi-step reaction with 5 steps

1: Vitride^? / toluene / 5 - 20 °C

2: N,N-dimethyl-formamide; pyridine / 20 - 60 °C

3: (S)-Mandelic acid / tert-Amyl alcohol / 70 °C

4: triethylamine; pyridine / dichloromethane / 10 - 20 °C

5: hydrogenchloride / water; acetonitrile / 1 h / 50 °C / pH 2 - 2.5

With pyridine; hydrogenchloride; (S)-Mandelic acid; triethylamine; In pyridine; tert-Amyl alcohol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;