(R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol

Base Information

• Chemical Name: (R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol
• CAS No.: 1539220-53-5
• Molecular Formula: C₄₁H₄₅NO₂
• Molecular Weight: 583.814

Synonyms:(R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol

Chemical Property of (R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol

Chemical Property:

Purity/Quality:

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Technology Process of (R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol

There total 12 articles about (R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

(R,S)-3-(2-hydroxy-5-(trityloxymethyl)phenyl)-N,N-diisopropyl-3-phenylpropanamide (1539220-76-2) → (R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol (1539220-53-5)

Guidance literature:

With Vitride; In toluene; at 5 - 25 ℃; Inert atmosphere; Cooling with ice;

Reference yield: 67.0%

(R)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol (1539221-44-7) → (R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol (1539220-53-5)

Guidance literature:

With sodium amide; methoxybenzene; at 90 - 125 ℃; for 3h; Concentration;

Reference yield: 58.0%

(R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-hydroxymethylphenol hydrochloride (250214-40-5) + trityl chloride (76-83-5) → (R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol (1539220-53-5)

Guidance literature:

In pyridine; N,N-dimethyl-formamide; at 20 - 60 ℃;

upstream raw materials:

ethyl (R,S)-3-(3-N,N-(diisopropylamino)-3-oxo-1-phenylpropyl)-4-hydroxybenzoate

(R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-hydroxymethylphenol hydrochloride

trityl chloride

(R)-2-[3-(diisopropylamino)-1-phenylpropyl]-4-(hydroxymethyl)-phenol

Downstream raw materials:

(R,S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-hydroxymethylphenol hydrochloride

(R)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol

(S)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-trityloxymethylphenol

(R)-2-(3-N,N-diisopropylamino-1-phenylpropyl)-4-hydroxymethylphenol hydrochloride

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