(+/-)-1,2,4/3-1,4-Di-O-benzyl-2,3-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol

Base Information

• Chemical Name: (+/-)-1,2,4/3-1,4-Di-O-benzyl-2,3-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol
• CAS No.: 129662-35-7
• Molecular Formula: C₂₈H₃₈O₈
• Molecular Weight: 502.605

Synonyms:(+/-)-1,2,4/3-1,4-Di-O-benzyl-2,3-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol

Chemical Property of (+/-)-1,2,4/3-1,4-Di-O-benzyl-2,3-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol

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Technology Process of (+/-)-1,2,4/3-1,4-Di-O-benzyl-2,3-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol

There total 8 articles about (+/-)-1,2,4/3-1,4-Di-O-benzyl-2,3-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(1S,4S,5R,6R)-5,6-Bis-(2-methoxy-ethoxymethoxy)-cyclohex-2-ene-1,4-diol (129662-34-6,130659-81-3) + benzyl bromide (100-39-0) → C28H38O8 (129662-35-7)

Guidance literature:

With sodium hydride;

DOI:10.1016/S0040-4039(00)97419-7

Reference yield: 67.0%

(+/-)-1,2,4/3-2,3-Di-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol (129662-34-6,130659-81-3) + benzyl bromide (100-39-0) → (+/-)-1,2,4/3-1,4-Di-O-benzyl-2,3-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol (129662-35-7)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 2h;

DOI:10.1016/0008-6215(92)85049-6

Reference yield: 64.0%

(+/-)-1,2,4/3-2,3-Di-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol (129662-34-6,130659-81-3) → (+/-)-1,2,4/3-1,4-Di-O-benzyl-2,3-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol (129662-35-7)

Guidance literature:

benzylation;

DOI:10.1016/0040-4039(90)80032-H

upstream raw materials:

(+/-)-1,2,4/3-2,3-Di-O-(2-methoxyethoxymethyl)cyclohex-5-ene-1,2,3,4-tetrol

benzyl bromide

(1RS,2RS)-cyclohexa-3,5-diene-1,2-diol

trans-1,2-Di-O-(2-methoxyethoxymethyl)cyclohexa-3,5-diene-1,2-diol

Downstream raw materials:

(+/-)-1,4-Di-O-benzyl-2,3,5-tri-O-(2-methoxyethoxymethyl)-chiro-inositol

(1S,2R,3S,4S,5R,6S)-2,5-Bis-benzyloxy-3,4,6-tris-(2-methoxy-ethoxymethoxy)-cyclohexanol

(1R,2R,3S,4S,5R,6R)-2,5-Bis-benzyloxy-3,4,6-tris-(2-methoxy-ethoxymethoxy)-cyclohexanol

rac-1,2,3,4-Tetra-O-benzyl-myo-inositol

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