[Au(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)(2,2'-bipyridine)][AuCl₂(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)]

Base Information

• Chemical Name: [Au(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)(2,2'-bipyridine)][AuCl₂(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)]
• CAS No.: 88291-90-1
• Molecular Formula: C₂₈H₂₀AuCl₂*C₃₈H₂₈AuN₂
• Molecular Weight: 1333.96

Synonyms:[Au(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)(2,2'-bipyridine)][AuCl₂(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)]

Chemical Property of [Au(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)(2,2'-bipyridine)][AuCl₂(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)]

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Technology Process of [Au(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)(2,2'-bipyridine)][AuCl₂(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)]

There total 1 articles about [Au(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)(2,2'-bipyridine)][AuCl₂(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-chloro-2,3,4,5-tetraphenylaura-cyclopentadiene dimer (71534-81-1) → [Au(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)(2,2'-bipyridine)][AuCl2(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)] (88291-90-1)

Guidance literature:

With 2,2'-bipyridyl; In dichloromethane; ligand added to suspn. of Au complex in CH2Cl2, stirred at room temp. for 4 h; concd., Et2O slowly added, ppt. filtered off, washed with Et2O, dried in vac.; elem. anal.;

DOI:10.1039/DT9830001131

Reference yield: 80.0%

sodium perchlorate monohydrate (7791-07-3) + [Au(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)(2,2'-bipyridine)][AuCl2(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)] (88291-90-1) → (2,2'-bipyridine)(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)gold(III) perchlorate (88291-76-3)

Guidance literature:

With 2,2'-bipyridyl; In acetone; bipy and NaClO4*H2O added to suspn. of Au complex in acetone, stirred at room temp. for 6 h; evapd., extd. with CH2Cl2, filtered, concd., Et2O added slowly, ppt. recrystd. from CH2Cl2-Et2O; elem. anal.;

DOI:10.1039/DT9830001131

upstream raw materials:

1-chloro-2,3,4,5-tetraphenylaura-cyclopentadiene dimer

Downstream raw materials:

(2,2'-bipyridine)(1,2,3,4-tetraphenylbuta-1,3-diene-1,4-diyl)gold(III) perchlorate

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