1-phenyl-1,2,3,4-tetrahydroarsinoline

Base Information

Chemical Name:1-phenyl-1,2,3,4-tetrahydroarsinoline
CAS No.:1082-13-9
Molecular Formula:C₁₅H₁₅As
Molecular Weight:270.206
Hs Code.:

Synonyms:1-phenyl-1,2,3,4-tetrahydroarsinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenyl-1,2,3,4-tetrahydroarsinoline

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Technology Process of 1-phenyl-1,2,3,4-tetrahydroarsinoline

There total 2 articles about 1-phenyl-1,2,3,4-tetrahydroarsinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1075-28-1
1-bromo-2-(3-bromopropyl)benzene

: 1087-49-6
1,6-diphenylhexane

: 1082-13-9
1-phenyl-1,2,3,4-tetrahydroarsinoline

Guidance literature:: 1-bromo-2-(3-bromopropyl)benzene; With magnesium; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere;

phenylarsine oxide; In tetrahydrofuran; at 0 - 20 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.jorganchem.2015.03.006

Reference yield:

: 1082-13-9
1-phenyl-1,2,3,4-tetrahydroarsinoline

Guidance literature:: Aus 1) Phenyl-(3-phenyl-propyl)-arsinsaeure in konz. H2SO4 (100grad,15min), dann 2) Rk.produkt in CHCl3 unter wssr. HCl (KI) mit gasf. SO2 (2h);