Benzene, 1-bromo-2-(3-bromopropyl)-

Base Information

• Chemical Name: Benzene, 1-bromo-2-(3-bromopropyl)-
• CAS No.: 1075-28-1
• Molecular Formula: C9H10Br2
• Molecular Weight: 277.986
• Mol file: 1075-28-1.mol

Synonyms:

Chemical Property of Benzene, 1-bromo-2-(3-bromopropyl)-

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzene, 1-bromo-2-(3-bromopropyl)-

There total 8 articles about Benzene, 1-bromo-2-(3-bromopropyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

3-(2-bromo-phenyl)-propan-1-ol (52221-92-8) → 1-bromo-2-(3-bromopropyl)benzene (1075-28-1)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/adsc.201901322

Reference yield: 82.0%

1-allyl-2-bromobenzene (42918-20-7) → 1-bromo-2-(3-bromopropyl)benzene (1075-28-1)

Guidance literature:

With hydrogen bromide; 3-chloro-benzenecarboperoxoic acid; In toluene; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/ejoc.200900096

Reference yield:

3-(2-bromophenyl)propionic acid (15115-58-9) → 1-Bromo-3-phenylpropane (637-59-2) + 1-bromo-2-(3-bromopropyl)benzene (1075-28-1)

Guidance literature:

3-(2-bromophenyl)propionic acid; With lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; at 75 ℃; for 1h;

With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 1h;

With lithium bromide; In acetone; for 8.5h; Further stages. Title compound not separated from byproducts.; Heating;

DOI:10.1002/anie.200702928

upstream raw materials:

3-(2-bromo-phenyl)-propan-1-ol

2-methylphenyl bromide

3-(2-bromophenyl)propionic acid

1-Bromo-2-bromomethyl-benzene

Downstream raw materials:

3-(2-bromophenyl)propyl methyl ether

[3-(2-Bromo-phenyl)-propyl]-phosphonic acid diethyl ester

2-{1-[3-(2-Bromo-phenyl)-propyl]-1H-indol-3-yl}-N,N-dipropyl-acetamide

Ethyl 1-<3-(2-Bromophenyl)propyl>-2-oxocyclohexane-1-carboxylate