(dimethyl(phenyl)silyl)zinc chloride

Base Information

Chemical Name:(dimethyl(phenyl)silyl)zinc chloride
CAS No.:1234935-78-4
Molecular Formula:C₈H₁₁ClSiZn
Molecular Weight:236.104
Hs Code.:

Synonyms:(dimethyl(phenyl)silyl)zinc chloride

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Chemical Property of (dimethyl(phenyl)silyl)zinc chloride

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Technology Process of (dimethyl(phenyl)silyl)zinc chloride

There total 2 articles about (dimethyl(phenyl)silyl)zinc chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 768-33-2
phenyldimethylsilyl chloride

: 7646-85-7,24359-56-6
zinc(II) chloride

: 1234935-78-4
(dimethyl(phenyl)silyl)zinc chloride

Guidance literature:: phenyldimethylsilyl chloride; With lithium; In tetrahydrofuran; at 0 - 10 ℃; for 13h; Inert atmosphere; Sonication;

zinc(II) chloride; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.6b03465

Reference yield:

: 3839-31-4
dimethyl(phenyl)silyl lithium

: 7646-85-7,24359-56-6
zinc(II) chloride

: 1234935-78-4
(dimethyl(phenyl)silyl)zinc chloride

Guidance literature:: In tetrahydrofuran;
DOI:10.1002/adsc.201900949

Reference yield: 97.0%

: 1234935-78-4
(dimethyl(phenyl)silyl)zinc chloride

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 79328-17-9
3-dimethylphenylsilyl-1-phenyl-1-propene

Guidance literature:: (2E)-3-phenyl-2-propen-1-ol; With dichlorobis(trimethylphosphine)nickel; methylzinc chloride; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

(dimethyl(phenyl)silyl)zinc chloride; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;

In toluene; at 20 ℃; for 5h; Reagent/catalyst; Solvent; Temperature; regioselective reaction; Catalytic behavior; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.9b02946