((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methanol

Base Information

• Chemical Name: ((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methanol
• CAS No.: 1233959-56-2
• Molecular Formula: C₂₀H₂₂O₄
• Molecular Weight: 326.392

Synonyms:((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methanol

Chemical Property of ((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methanol

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Technology Process of ((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methanol

There total 1 articles about ((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl(((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methoxy)dimethylsilane (1233959-33-5) → ((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methanol (1233959-56-2)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; Inert atmosphere;

DOI:10.1021/ol101144k

Reference yield: 94.0%

((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methanol (1233959-56-2) + methyl iodide (74-88-4) → (2R,3S,6S)-3-(3-methoxybenzyloxy)-2-(methoxymethyl)-6-phenyl-3,6-dihydro-2H-pyran (1233959-60-8)

Guidance literature:

With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1021/ol101144k

Reference yield: 85.0%

((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methanol (1233959-56-2) + acetic anhydride (108-24-7) → ((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methyl acetate (1233959-34-6)

Guidance literature:

With pyridine; dmap; In dichloromethane; at 20 ℃; for 6h; Inert atmosphere;

DOI:10.1021/ol101144k

upstream raw materials:

tert-butyl(((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methoxy)dimethylsilane

Downstream raw materials:

(2S,3S,6S)-2-(bromomethyl)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran

((2R,3S,6S)-3-(3-methoxybenzyloxy)-6-phenyl-3,6-dihydro-2H-pyran-2-yl)methyl acetate

(2R,3S,6S)-3-(3-methoxybenzyloxy)-2-(methoxymethyl)-6-phenyl-3,6-dihydro-2H-pyran

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