(6S,10S)-3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione

Base Information

Chemical Name:(6S,10S)-3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione
CAS No.:1397692-16-8
Molecular Formula:C₂₆H₂₁NO₂S₂
Molecular Weight:443.59
Hs Code.:

Synonyms:(6S,10S)-3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione

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Chemical Property of (6S,10S)-3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione

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Technology Process of (6S,10S)-3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione

There total 3 articles about (6S,10S)-3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 13037-56-4
5-benzylidene-3-phenyl-2-thioxothiazolidin-4-one

: 122-57-6
1-Phenylbut-1-en-3-one

: 1397692-16-8
(6S,10S)-3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione

Guidance literature:: With (S)-N¹-cyclohexyl-3,3-dimethylbutane-1,2-diamine; Boc-Trp-OH; In chloroform; at 50 ℃; for 48h; optical yield given as %ee; stereoselective reaction;
DOI:10.1039/c2cc34321e

Reference yield:

: 1457-46-1
3-phenylrhodanine

: 538-58-9
1,5-diphenyl-1,4-pentadiene-3-one

: 1397692-16-8
(6S,10S)-3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione

: 3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione

Guidance literature:: With C₂₀H₂₅N₃O; 2,4-dinitrobenzoic acid; In acetonitrile; at 40 ℃; for 96h; Time; Temperature; Overall yield = 83 %; stereoselective reaction; Catalytic behavior;
DOI:10.1002/ejoc.201300931

Reference yield:

: 1457-46-1
3-phenylrhodanine

: 538-58-9
1,5-diphenyl-1,4-pentadiene-3-one

: 1397692-16-8
(6S,10S)-3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione

: 3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione

: 3,6,10-triphenyl-2-thioxo-1-thia-3-azaspiro[4.5]decane-4,8-dione

Guidance literature:: With 2,4-dinitrobenzoic acid; 9-amino-(9-deoxy)epi-cinchonidine; In tetrahydrofuran; at 20 ℃; for 312h; Reagent/catalyst; Overall yield = 82 %; stereoselective reaction;
DOI:10.1002/ejoc.201300931