C₇₇H₉₇NO₈S

Base Information

Chemical Name:C₇₇H₉₇NO₈S
CAS No.:946073-27-4
Molecular Formula:C₇₇H₉₇NO₈S
Molecular Weight:1196.69
Hs Code.:

C<sub>77</sub>H<sub>97</sub>NO<sub>8</sub>S

Synonyms:C₇₇H₉₇NO₈S

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Chemical Property of C₇₇H₉₇NO₈S

Chemical Property:

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Technology Process of C₇₇H₉₇NO₈S

There total 14 articles about C₇₇H₉₇NO₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 946073-46-7
C₆₉H₉₁NO₇

: 69746-43-6
1-iodo-4-thioacetylbenzene

: 946073-27-4
C₇₇H₉₇NO₈S

Guidance literature:: With copper(l) iodide; triethylamine; triphenylphosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; chloroform; at 20 ℃; for 48h;
DOI:10.1016/j.tet.2007.05.006

Reference yield:

: 153033-31-9
1,4-bis(hexyloxy)-2,5-diiodobenzene

: 946073-27-4
C₇₇H₉₇NO₈S

Guidance literature:: Multi-step reaction with 10 steps

1.1: PPh₃; pyridine; triethylamine / CuI; Pd₂(dba)3 / CHCl₃ / 0.17 h

1.2: 50 percent / CHCl₃ / 48 h / 75 °C

2.1: 87 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 70 °C

3.1: 79 percent / NaOH / toluene / 24 h / Heating

4.1: 86 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 75 °C

5.1: 93 percent / TBAF / tetrahydrofuran / 20 °C

6.1: 38 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 65 - 70 °C

7.1: 99 percent / TBAF / tetrahydrofuran / 20 °C

8.1: 40 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 75 °C

9.1: 90 percent / TBAF / tetrahydrofuran / 20 °C

10.1: 66 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃; tetrahydrofuran / 48 h / 20 °C

With pyridine; sodium hydroxide; copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; copper(l) iodide; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; chloroform; toluene; 2.1: Sonogashira coupling / 4.1: Sonogashira coupling / 6.1: Sonogashira coupling / 8.1: Sonogashira coupling / 10.1: Sonogashira coupling;
DOI:10.1016/j.tet.2007.05.006

Reference yield:

: 830336-55-5
(2,5-bis-hexyloxy-4-iodo-phenylethynyl)-triisopropyl-silane

: 946073-27-4
C₇₇H₉₇NO₈S

Guidance literature:: Multi-step reaction with 5 steps

1: 38 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 65 - 70 °C

2: 99 percent / TBAF / tetrahydrofuran / 20 °C

3: 40 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃ / 48 h / 75 °C

4: 90 percent / TBAF / tetrahydrofuran / 20 °C

5: 66 percent / PPh₃; triethylamine; CuI / Pd₂(dba)3 / CHCl₃; tetrahydrofuran / 48 h / 20 °C

With copper(l) iodide; tetrabutyl ammonium fluoride; triethylamine; triphenylphosphine; tris(dibenzylideneacetone)dipalladium ⁽⁰⁾; In tetrahydrofuran; chloroform; 1: Sonogashira coupling / 3: Sonogashira coupling / 5: Sonogashira coupling;
DOI:10.1016/j.tet.2007.05.006