sodium 2,2,3,4-tetraethyl-2,5-dihydro-5,5-diphenyl-1,2,5-oxoniadiboratolate

Base Information

Chemical Name:sodium 2,2,3,4-tetraethyl-2,5-dihydro-5,5-diphenyl-1,2,5-oxoniadiboratolate
CAS No.:138517-83-6
Molecular Formula:C₂₂H₃₁B₂O*Na
Molecular Weight:356.099
Hs Code.:

Synonyms:sodium 2,2,3,4-tetraethyl-2,5-dihydro-5,5-diphenyl-1,2,5-oxoniadiboratolate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium 2,2,3,4-tetraethyl-2,5-dihydro-5,5-diphenyl-1,2,5-oxoniadiboratolate

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Technology Process of sodium 2,2,3,4-tetraethyl-2,5-dihydro-5,5-diphenyl-1,2,5-oxoniadiboratolate

There total 1 articles about sodium 2,2,3,4-tetraethyl-2,5-dihydro-5,5-diphenyl-1,2,5-oxoniadiboratolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 138517-72-3
(Z)-3-(diethylboryl)-4-(diphenylboryl)-3-hexene

: 1310-73-2
sodium hydroxide

: 138517-83-6
sodium 2,2,3,4-tetraethyl-2,5-dihydro-5,5-diphenyl-1,2,5-oxoniadiboratolate

Guidance literature:: In toluene; Ar atmosphere; addn. of B-compd. in toluene to suspn. of NaOH in toluene (50 min), stirring (6 h, room temp.); removal of solvent (0.001 Torr), addn. of pentane, stirring (several h, room temp.), filtration, drying (0.001 Torr); elem. anal.;