diethyl 2-benzyloxycarbonylamino-2-malonate

Base Information

Chemical Name:diethyl 2-benzyloxycarbonylamino-2-malonate
CAS No.:129243-63-6
Molecular Formula:C₂₅H₃₂N₂O₈
Molecular Weight:488.538
Hs Code.:

diethyl 2-benzyloxycarbonylamino-2-<N-(t-butoxycarbonyl)-pyrrol-2-ylmethyl>malonate

Synonyms:diethyl 2-benzyloxycarbonylamino-2-malonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl 2-benzyloxycarbonylamino-2-malonate

Chemical Property:

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Technology Process of diethyl 2-benzyloxycarbonylamino-2-malonate

There total 5 articles about diethyl 2-benzyloxycarbonylamino-2-malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 129243-62-5
diethyl 2-benzyloxycarbonylamino-2-pyrrol-2-ylmethylmalonate

: 129243-63-6
diethyl 2-benzyloxycarbonylamino-2-malonate

Guidance literature:: With dmap; In acetonitrile; for 16h; Ambient temperature;

Reference yield:

: 3072-56-8
2-(diethylaminomethyl)pyrrole

: 129243-63-6
diethyl 2-benzyloxycarbonylamino-2-malonate

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / ethanol / 2 h

2: 1) Na, EtOH / 2) reflux, 2h

3: 97 percent / dimethylaminopyridine / acetonitrile / 16 h / Ambient temperature

With dmap; ethanol; sodium; In ethanol; acetonitrile;

Reference yield:

: 13433-00-6
diethyl aminomalonate hydrochloride

: 129243-63-6
diethyl 2-benzyloxycarbonylamino-2-malonate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NEt₃ / CH₂Cl₂ / 1) 0 deg C, 10 min, 2) RT, 1h

2: 1) Na, EtOH / 2) reflux, 2h

3: 97 percent / dimethylaminopyridine / acetonitrile / 16 h / Ambient temperature

With dmap; ethanol; sodium; triethylamine; In dichloromethane; acetonitrile;