(3S,4S,5S)-3-((4-methoxyphenoxy)methyl)-5-nitro-4-phenylcyclohex-1-ene carbaldehyde

Base Information

Chemical Name:(3S,4S,5S)-3-((4-methoxyphenoxy)methyl)-5-nitro-4-phenylcyclohex-1-ene carbaldehyde
CAS No.:1186430-90-9
Molecular Formula:C₂₁H₂₁NO₅
Molecular Weight:367.401
Hs Code.:

Synonyms:(3S,4S,5S)-3-((4-methoxyphenoxy)methyl)-5-nitro-4-phenylcyclohex-1-ene carbaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S,4S,5S)-3-((4-methoxyphenoxy)methyl)-5-nitro-4-phenylcyclohex-1-ene carbaldehyde

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Technology Process of (3S,4S,5S)-3-((4-methoxyphenoxy)methyl)-5-nitro-4-phenylcyclohex-1-ene carbaldehyde

There total 2 articles about (3S,4S,5S)-3-((4-methoxyphenoxy)methyl)-5-nitro-4-phenylcyclohex-1-ene carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 102-96-5
(2-nitroethenyl)benzene

: 479192-15-9
3-(4-methoxyphenoxy)propionaldehyde

: 1186430-90-9
(3S,4S,5S)-3-((4-methoxyphenoxy)methyl)-5-nitro-4-phenylcyclohex-1-ene carbaldehyde

Guidance literature:: With (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; In hexane; at 0 ℃; for 24h; stereoselective reaction;
DOI:10.1016/j.tetlet.2017.05.002

Reference yield: 51.0%

: 102-96-5
(2-nitroethenyl)benzene

: 150-76-5
4-methoxy-phenol

: 107-02-8,25068-14-8
acrolein

: 1186430-90-9
(3S,4S,5S)-3-((4-methoxyphenoxy)methyl)-5-nitro-4-phenylcyclohex-1-ene carbaldehyde

Guidance literature:: With (2S)-2-{diphenyl[(trimethylsilyl)oxy]methyl}pyrrolidine; In chloroform; at 4 - 20 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/chem.200900613