C₃₆H₆₇NO₃

Base Information

• Chemical Name: C₃₆H₆₇NO₃
• CAS No.: 1318253-53-0
• Molecular Formula: C₃₆H₆₇NO₃
• Molecular Weight: 561.933
• Mol file: 1318253-53-0.mol

Synonyms:C₃₆H₆₇NO₃

Chemical Property of C₃₆H₆₇NO₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₆₇NO₃

There total 9 articles about C₃₆H₆₇NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4,5-tris((R)-3,7-dimethyloctyloxy)benzoic acid chloride → C36H67NO3 (1318253-53-0)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium azide / tetrahydrofuran; water / 0 - 20 °C

2: 1,4-dioxane / 0.5 h / Reflux

3: tetra(n-butyl)ammonium hydroxide / 1,4-dioxane; water / 0.25 h / 90 °C

With sodium azide; tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; 1,4-dioxane; water;

DOI:10.1021/ja204543f

Reference yield:

3,4,5-tris((R)-3,7-dimethyloctyloxy)benzoic acid methyl ester (1318253-54-1) → C36H67NO3 (1318253-53-0)

Guidance literature:

Multi-step reaction with 5 steps

1: sodium hydroxide / ethanol / 8 h / Reflux

2: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.75 h / 0 °C

3: sodium azide / tetrahydrofuran; water / 0 - 20 °C

4: 1,4-dioxane / 0.5 h / Reflux

5: tetra(n-butyl)ammonium hydroxide / 1,4-dioxane; water / 0.25 h / 90 °C

With sodium azide; tetra(n-butyl)ammonium hydroxide; chloroformic acid ethyl ester; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; water;

DOI:10.1021/ja204543f

Reference yield:

dihydro-(R)-(+)-β-citronellyl tosylate (59965-19-4) → C36H67NO3 (1318253-53-0)

Guidance literature:

Multi-step reaction with 6 steps

1: tetrabutylammomium bromide; potassium carbonate / acetone / Inert atmosphere; Reflux

2: sodium hydroxide / ethanol / 8 h / Reflux

3: chloroformic acid ethyl ester; triethylamine / tetrahydrofuran / 0.75 h / 0 °C

4: sodium azide / tetrahydrofuran; water / 0 - 20 °C

5: 1,4-dioxane / 0.5 h / Reflux

6: tetra(n-butyl)ammonium hydroxide / 1,4-dioxane; water / 0.25 h / 90 °C

With sodium azide; tetrabutylammomium bromide; tetra(n-butyl)ammonium hydroxide; chloroformic acid ethyl ester; potassium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; ethanol; water; acetone;

DOI:10.1021/ja204543f

upstream raw materials:

3,4,5-tris((R)-3,7-dimethyloctyloxy)benzoic acid methyl ester

(3R)-citronellol

dihydro-(R)-(+)-β-citronellyl tosylate

(R)-3,7-dimethyloctan-1-ol