dimethyl 4-({methoxycarbonyl-[3-(2-methyl-[1,3]dioxolan-2-yl)phenyl]amino}methyl)phthalate

Base Information

Chemical Name:dimethyl 4-({methoxycarbonyl-[3-(2-methyl-[1,3]dioxolan-2-yl)phenyl]amino}methyl)phthalate
CAS No.:268234-36-2
Molecular Formula:C₂₃H₂₅NO₈
Molecular Weight:443.453
Hs Code.:

Synonyms:dimethyl 4-({methoxycarbonyl-[3-(2-methyl-[1,3]dioxolan-2-yl)phenyl]amino}methyl)phthalate

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Chemical Property of dimethyl 4-({methoxycarbonyl-[3-(2-methyl-[1,3]dioxolan-2-yl)phenyl]amino}methyl)phthalate

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Technology Process of dimethyl 4-({methoxycarbonyl-[3-(2-methyl-[1,3]dioxolan-2-yl)phenyl]amino}methyl)phthalate

There total 1 articles about dimethyl 4-({methoxycarbonyl-[3-(2-methyl-[1,3]dioxolan-2-yl)phenyl]amino}methyl)phthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 20116-67-0
4-bromomethylphthalic acid dimethyl ester

: 51226-14-3
2-(3-amino)phenyl-2-methyl-1,3-dioxolane

: 79-22-1
methyl chloroformate

: 268234-36-2
dimethyl 4-({methoxycarbonyl-[3-(2-methyl-[1,3]dioxolan-2-yl)phenyl]amino}methyl)phthalate

Guidance literature:: 2-(3-amino)phenyl-2-methyl-1,3-dioxolane; methyl chloroformate; With zinc; In toluene; at 20 ℃; for 1h;

With sodium hydride; In DMF (N,N-dimethyl-formamide); at 0 ℃; for 0.5h;

4-bromomethylphthalic acid dimethyl ester; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 2h;

Reference yield: 91.0%

: 268234-36-2
dimethyl 4-({methoxycarbonyl-[3-(2-methyl-[1,3]dioxolan-2-yl)phenyl]amino}methyl)phthalate

: 268234-37-3
1-{3-[(3,4-bis-hydroxymethylbenzyl)methylamino]-phenyl}ethanone

Guidance literature:: dimethyl 4-({methoxycarbonyl-[3-(2-methyl-[1,3]dioxolan-2-yl)phenyl]amino}methyl)phthalate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 4h; Heating / reflux;

With sulfuric acid; In methanol; for 24h;