Technology Process of C31H32N3O7P
There total 12 articles about C31H32N3O7P which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3-[4-(2-cyanophenoxy)anilino]-4-(3-hydroxyphenyl)-2,5-dioxo-2,5-dihydro-lH-pyrrole; di-tert-butyl N,N-diethylphosphoramidite;
In
tetrahydrofuran;
at 20 ℃;
for 2h;
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
at -60 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: ammonium hydroxide / water / 0 - 20 °C
2.1: potassium carbonate / DMF (N,N-dimethyl-formamide) / 20 °C
3.1: potassium tert-butylate / DMF (N,N-dimethyl-formamide) / 1 h / -10 - 20 °C
4.1: thionyl chloride / DMF (N,N-dimethyl-formamide); dichloromethane / 3 h / 20 °C
5.1: cyclohexanol / 120 °C
6.1: hydrogen / Pearlman's catalyst / ethanol; ethyl acetate / 5 h
7.1: tetrahydrofuran / 2 h / 20 °C
7.2: 0.5 h / -60 °C
With
thionyl chloride; potassium tert-butylate; hydrogen; potassium carbonate; ammonium hydroxide;
Pearlman's catalyst;
In
tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; dichloromethane; water; ethyl acetate; cyclohexanol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: hydrogen / Pearlman's catalyst / ethanol; ethyl acetate / 5 h
2.1: tetrahydrofuran / 2 h / 20 °C
2.2: 0.5 h / -60 °C
With
hydrogen;
Pearlman's catalyst;
In
tetrahydrofuran; ethanol; ethyl acetate;
![3-[4-(2-cyanophenoxy)anilino]-4-(3-hydroxyphenyl)-2,5-dioxo-2,5-dihydro-lH-pyrrole](/Databaselist/images/loading.webp)
