N-phenyl-C-styrylmethanohydrazonyl bromide

Base Information

• Chemical Name: N-phenyl-C-styrylmethanohydrazonyl bromide
• CAS No.: 129200-94-8
• Molecular Formula: C₁₅H₁₃BrN₂
• Molecular Weight: 301.186

Synonyms:N-phenyl-C-styrylmethanohydrazonyl bromide

Chemical Property of N-phenyl-C-styrylmethanohydrazonyl bromide

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Technology Process of N-phenyl-C-styrylmethanohydrazonyl bromide

There total 1 articles about N-phenyl-C-styrylmethanohydrazonyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

3-phenylacrylic acid N'-phenylhydrazide (129200-93-7) → N-phenyl-C-styrylmethanohydrazonyl bromide (129200-94-8)

Guidance literature:

With carbon tetrabromide; triphenylphosphine; In acetonitrile; for 1h;

Reference yield: 98.0%

N-phenyl-C-styrylmethanohydrazonyl bromide (129200-94-8) + 2,3,4,6-tetra-O-acetyl-1-thio-α-D-glucopyranose (92691-83-3) → 2,3,4,6-tetra-O-acetyl-1-S-(N-phenylcinnamohydrazonoyl)-1-thio-α-D-glucopyranose

Guidance literature:

With triethylamine; In diethyl ether; dichloromethane; for 1h; Ambient temperature;

Reference yield: 95.0%

tetraacetyl thioglucose (19879-84-6) + N-phenyl-C-styrylmethanohydrazonyl bromide (129200-94-8) → 2,3,4,6-tetra-O-acetyl-1-S-(N-phenylcinnamohydrazonoyl)-1-thio-β-D-glucopyranose

Guidance literature:

With triethylamine; In diethyl ether; dichloromethane; for 1h; Ambient temperature;

upstream raw materials:

3-phenylacrylic acid N'-phenylhydrazide

Downstream raw materials:

(3aR,6aR)-1,5-Diphenyl-3-((E)-styryl)-3a,6a-dihydro-1H-pyrrolo[3,4-c]pyrazole-4,6-dione

(3aR,6aR)-1-Phenyl-3-((E)-styryl)-5-p-tolyl-3a,6a-dihydro-1H-pyrrolo[3,4-c]pyrazole-4,6-dione

(3aR,6aR)-5-(4-Chloro-phenyl)-1-phenyl-3-((E)-styryl)-3a,6a-dihydro-1H-pyrrolo[3,4-c]pyrazole-4,6-dione

(3aR,6aR)-5-(4-Methoxy-phenyl)-1-phenyl-3-((E)-styryl)-3a,6a-dihydro-1H-pyrrolo[3,4-c]pyrazole-4,6-dione

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