2-(3-(t-butoxymethyl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane

Base Information

• Chemical Name: 2-(3-(t-butoxymethyl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane
• CAS No.: 1415046-66-0
• Molecular Formula: C₁₆H₂₅BO₃
• Molecular Weight: 276.184
• Mol file: 1415046-66-0.mol

Synonyms:2-(3-(t-butoxymethyl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane

Chemical Property of 2-(3-(t-butoxymethyl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2-(3-(t-butoxymethyl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane

There total 1 articles about 2-(3-(t-butoxymethyl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(3-(tert-butoxymethyl)phenyl)boronic acid (858364-78-0) + 2,2-Dimethyl-1,3-propanediol (126-30-7) → 2-(3-(t-butoxymethyl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane (1415046-66-0)

Guidance literature:

In tetrahydrofuran; for 0.666667h; Dean-Stark; Reflux;

DOI:10.1002/adsc.201400147

Reference yield: 97.0%

2-(3-(t-butoxymethyl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane (1415046-66-0) + 1-methoxynaphthalene-2-carboxylic acid diethylamide (404574-87-4) → 1-(3-(t-butoxymethyl)phenyl)-N,N-diethyl-2-naphthamide (1415045-85-0)

Guidance literature:

With carbonyl bis(hydrido)tris(triphenylphosphine)ruthenium(II); In toluene; for 20h; Inert atmosphere; Reflux; Sealed tube;

DOI:10.1021/acs.orglett.5b01913

Reference yield: 93.0%

2-(3-(t-butoxymethyl)phenyl)-5,5-dimethyl-1,3,2-dioxaborinane (1415046-66-0) + N,N-diethylfuran-3-carboxamide (73540-76-8) → N,N-diethyl-2-(3-(t-butoxymethyl)phenyl)furan-3-carboxamide (1415045-38-3)

Guidance literature:

With 3C₁₈H₁₅P*H₂ORh; In toluene; at 125 - 135 ℃; for 44h; Inert atmosphere;

DOI:10.1002/adsc.201400147

upstream raw materials:

(3-(tert-butoxymethyl)phenyl)boronic acid

2,2-Dimethyl-1,3-propanediol

Downstream raw materials:

N,N-diethyl-2-(3-(t-butoxymethyl)phenyl)furan-3-carboxamide

1-(3-(t-butoxymethyl)phenyl)-N,N-diethyl-2-naphthamide