1-cyclopropyl-4-[[1-(2,5-dichlorophenoxymethyl)cyclopropyl]carbonyl]-1,2,3,4-tetrahydroquinoxaline trifluoroacetate

Base Information

Chemical Name:1-cyclopropyl-4-[[1-(2,5-dichlorophenoxymethyl)cyclopropyl]carbonyl]-1,2,3,4-tetrahydroquinoxaline trifluoroacetate
CAS No.:1445981-42-9
Molecular Formula:C₂HF₃O₂*C₂₂H₂₂Cl₂N₂O₂
Molecular Weight:531.359
Hs Code.:

Synonyms:1-cyclopropyl-4-[[1-(2,5-dichlorophenoxymethyl)cyclopropyl]carbonyl]-1,2,3,4-tetrahydroquinoxaline trifluoroacetate

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Chemical Property of 1-cyclopropyl-4-[[1-(2,5-dichlorophenoxymethyl)cyclopropyl]carbonyl]-1,2,3,4-tetrahydroquinoxaline trifluoroacetate

Chemical Property:

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Technology Process of 1-cyclopropyl-4-[[1-(2,5-dichlorophenoxymethyl)cyclopropyl]carbonyl]-1,2,3,4-tetrahydroquinoxaline trifluoroacetate

There total 9 articles about 1-cyclopropyl-4-[[1-(2,5-dichlorophenoxymethyl)cyclopropyl]carbonyl]-1,2,3,4-tetrahydroquinoxaline trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 583-78-8
2,5-dichlorophenol

: 1445984-95-1
1-[[1-(chloromethyl)cyclopropyl]carbonyl]-4-cyclopropyl-1,2,3,4-tetrahydroquinoxaline

: 76-05-1
trifluoroacetic acid

: 1445981-42-9
1-cyclopropyl-4-[[1-(2,5-dichlorophenoxymethyl)cyclopropyl]carbonyl]-1,2,3,4-tetrahydroquinoxaline trifluoroacetate

Guidance literature:: 2,5-dichlorophenol; 1-[[1-(chloromethyl)cyclopropyl]carbonyl]-4-cyclopropyl-1,2,3,4-tetrahydroquinoxaline; With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 65 ℃;

trifluoroacetic acid; In acetonitrile;

Reference yield:

: 1224640-11-2
1-cyclopropyl-4-hydroxy-1,2,3,4-tetrahydroquinoxaline-2,3-dione

: 1445981-42-9
1-cyclopropyl-4-[[1-(2,5-dichlorophenoxymethyl)cyclopropyl]carbonyl]-1,2,3,4-tetrahydroquinoxaline trifluoroacetate

Guidance literature:: Multi-step reaction with 4 steps

1: triphenylphosphine / N,N-dimethyl-formamide / 2 h / 135 °C / Inert atmosphere

2: borane-THF / tetrahydrofuran / 4 h / 50 °C

3: triethylamine / dichloromethane / 20 °C

4: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 65 °C

With borane-THF; potassium carbonate; triethylamine; triphenylphosphine; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 1224640-12-3
1-cyclopropyl-1,2,3,4-tetrahydroquinoxaline-2,3-dione

: 1445981-42-9
1-cyclopropyl-4-[[1-(2,5-dichlorophenoxymethyl)cyclopropyl]carbonyl]-1,2,3,4-tetrahydroquinoxaline trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1: borane-THF / tetrahydrofuran / 4 h / 50 °C

2: triethylamine / dichloromethane / 20 °C

3: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 65 °C

With borane-THF; potassium carbonate; triethylamine; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;