(2R,3R,4R)-2,3,5-tris(benzyloxy)-4-hydroxypentanal O-(tertbutyldiphenylsilyl)oxime

Base Information

Chemical Name:(2R,3R,4R)-2,3,5-tris(benzyloxy)-4-hydroxypentanal O-(tertbutyldiphenylsilyl)oxime
CAS No.:537030-20-9
Molecular Formula:C₄₂H₄₇NO₅Si
Molecular Weight:673.924
Hs Code.:

Synonyms:(2R,3R,4R)-2,3,5-tris(benzyloxy)-4-hydroxypentanal O-(tertbutyldiphenylsilyl)oxime

Suppliers and Price of (2R,3R,4R)-2,3,5-tris(benzyloxy)-4-hydroxypentanal O-(tertbutyldiphenylsilyl)oxime

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Chemical Property of (2R,3R,4R)-2,3,5-tris(benzyloxy)-4-hydroxypentanal O-(tertbutyldiphenylsilyl)oxime

Chemical Property:

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Technology Process of (2R,3R,4R)-2,3,5-tris(benzyloxy)-4-hydroxypentanal O-(tertbutyldiphenylsilyl)oxime

There total 3 articles about (2R,3R,4R)-2,3,5-tris(benzyloxy)-4-hydroxypentanal O-(tertbutyldiphenylsilyl)oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 160549-10-0
2,3,5-tri-O-benzyl-D-arabinofuranose

: 537030-20-9
(2R,3R,4R)-2,3,5-tris(benzyloxy)-4-hydroxypentanal O-(tertbutyldiphenylsilyl)oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / NH₂OH*HCl; NaOMe / methanol

2: 92 percent / pyridine / 25 °C

With pyridine; hydroxylamine hydrochloride; sodium methylate; In methanol;
DOI:10.1002/hlca.200390248

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-arabinofuranose

: 537030-20-9
(2R,3R,4R)-2,3,5-tris(benzyloxy)-4-hydroxypentanal O-(tertbutyldiphenylsilyl)oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: MeOH; H₂SO₄; Na₂SO₄ / 21 h / 20 °C

1.2: KOH; Na₂SO₄ / 8 h / Heating

1.3: 50 percent / HCl; water; CH₃COOH / 60 - 70 °C

2.1: NH₂OH*HCl / pyridine / 24 h / 20 °C

2.2: pyridine / 18 h / 20 °C

With methanol; sulfuric acid; hydroxylamine hydrochloride; sodium sulfate; In pyridine;
DOI:10.1016/S0040-4039(03)00239-9

Reference yield:

: 100-44-7
benzyl chloride

: 537030-20-9
(2R,3R,4R)-2,3,5-tris(benzyloxy)-4-hydroxypentanal O-(tertbutyldiphenylsilyl)oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: MeOH; H₂SO₄; Na₂SO₄ / 21 h / 20 °C

1.2: KOH; Na₂SO₄ / 8 h / Heating

1.3: 50 percent / HCl; water; CH₃COOH / 60 - 70 °C

2.1: NH₂OH*HCl / pyridine / 24 h / 20 °C

2.2: pyridine / 18 h / 20 °C

With methanol; sulfuric acid; hydroxylamine hydrochloride; sodium sulfate; In pyridine;
DOI:10.1016/S0040-4039(03)00239-9