4-(2-chlorophenyl)-1-methyl-2-(methylthio)-5-cyano-6-oxo-1,6-dihydropyrimidine

Base Information

Chemical Name:4-(2-chlorophenyl)-1-methyl-2-(methylthio)-5-cyano-6-oxo-1,6-dihydropyrimidine
CAS No.:438586-15-3
Molecular Formula:C₁₃H₁₀ClN₃OS
Molecular Weight:291.761
Hs Code.:

Synonyms:4-(2-chlorophenyl)-1-methyl-2-(methylthio)-5-cyano-6-oxo-1,6-dihydropyrimidine

Suppliers and Price of 4-(2-chlorophenyl)-1-methyl-2-(methylthio)-5-cyano-6-oxo-1,6-dihydropyrimidine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 4-(2-chlorophenyl)-1-methyl-2-(methylthio)-5-cyano-6-oxo-1,6-dihydropyrimidine

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 4-(2-chlorophenyl)-1-methyl-2-(methylthio)-5-cyano-6-oxo-1,6-dihydropyrimidine

There total 1 articles about 4-(2-chlorophenyl)-1-methyl-2-(methylthio)-5-cyano-6-oxo-1,6-dihydropyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 131364-73-3
C₁₁H₆ClN₃OS

: 74-88-4
methyl iodide

: 438586-15-3
4-(2-chlorophenyl)-1-methyl-2-(methylthio)-5-cyano-6-oxo-1,6-dihydropyrimidine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 3h;
DOI:10.1016/j.ejmech.2011.02.052

Reference yield: 63.0%

: 438586-15-3
4-(2-chlorophenyl)-1-methyl-2-(methylthio)-5-cyano-6-oxo-1,6-dihydropyrimidine

: 438586-16-4
4-(2-chlorophenyl)-2-hydrazino-1-methyl-5-cyano-6-oxo-1,6-dihydropyrimidine

Guidance literature:: With hydrazine hydrate; In ethanol; for 6h; Reflux;
DOI:10.1016/j.ejmech.2011.02.052

Reference yield:

: 438586-15-3
4-(2-chlorophenyl)-1-methyl-2-(methylthio)-5-cyano-6-oxo-1,6-dihydropyrimidine

: 1299484-88-0
ethyl 5-amino-1-[4-(2-chlorophenyl)-5-cyano-1-methyl-6-oxo-1,6-dihydropyrimidin-2-yl]-1H-pyrazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 6 h / Reflux

2: acetic acid / ethanol / Reflux

With hydrazine hydrate; acetic acid; In ethanol;
DOI:10.1016/j.ejmech.2011.02.052