N-benzyl derivative of 5-carbethoxy,5,6-dimethyl-pyrido-<4,3-b>carbazol-(5H)-11-one

Base Information

Chemical Name:N-benzyl derivative of 5-carbethoxy,5,6-dimethyl-pyrido-<4,3-b>carbazol-(5H)-11-one
CAS No.:777010-83-0
Molecular Formula:C₂₇H₂₅N₂O₃
Molecular Weight:425.507
Hs Code.:

Synonyms:N-benzyl derivative of 5-carbethoxy,5,6-dimethyl-pyrido-<4,3-b>carbazol-(5H)-11-one

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Chemical Property of N-benzyl derivative of 5-carbethoxy,5,6-dimethyl-pyrido-<4,3-b>carbazol-(5H)-11-one

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Technology Process of N-benzyl derivative of 5-carbethoxy,5,6-dimethyl-pyrido-<4,3-b>carbazol-(5H)-11-one

There total 5 articles about N-benzyl derivative of 5-carbethoxy,5,6-dimethyl-pyrido-<4,3-b>carbazol-(5H)-11-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 81451-83-4,81451-84-5
2-benzyl-5-carbethoxy-5,6-dimethyl 4a,5-dihydropyrido<4,3,b>carbazol(5-H)-11-one

: 777010-83-0
N-benzyl derivative of 5-carbethoxy,5,6-dimethyl-pyrido-<4,3-b>carbazol-(5H)-11-one

Guidance literature:: With 10-benzylacridin-10-ium bromide; In acetonitrile; for 1h; Ambient temperature;
DOI:10.1016/S0040-4020(01)88606-3

Reference yield:

: 603-76-9
1-methylindole

: 777010-83-0
N-benzyl derivative of 5-carbethoxy,5,6-dimethyl-pyrido-<4,3-b>carbazol-(5H)-11-one

Guidance literature:: Multi-step reaction with 6 steps

1: 63 percent / n-BuLi / tetrahydrofuran / 1 h

2: POCl₃ / pyridine / 1.) room temp, 1 h, 2:) 75 deg C, 1.5 h

3: NaBH₄ / ethanol / 2 h

4: 55 percent / tetrahydrothiophene 1,1-dioxide / 0.5 h / 120 °C

5: 2.) Et₃N / 1.) CH₃Cl, r.t.; 2.) EtOAc, r.t.

6: 90 percent / N-benzyl acridinium bromide / acetonitrile / 1 h / Ambient temperature

With sodium tetrahydroborate; n-butyllithium; 10-benzylacridin-10-ium bromide; triethylamine; trichlorophosphate; In tetrahydrofuran; pyridine; sulfolane; ethanol; acetonitrile;
DOI:10.1016/S0040-4020(01)88606-3

Reference yield:

: 72938-66-0
Ethyl α-(N-methylindol-2-yl)acrylate

: 777010-83-0
N-benzyl derivative of 5-carbethoxy,5,6-dimethyl-pyrido-<4,3-b>carbazol-(5H)-11-one

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₄ / ethanol / 2 h

2: 55 percent / tetrahydrothiophene 1,1-dioxide / 0.5 h / 120 °C

3: 2.) Et₃N / 1.) CH₃Cl, r.t.; 2.) EtOAc, r.t.

4: 90 percent / N-benzyl acridinium bromide / acetonitrile / 1 h / Ambient temperature

With sodium tetrahydroborate; 10-benzylacridin-10-ium bromide; triethylamine; In sulfolane; ethanol; acetonitrile;
DOI:10.1016/S0040-4020(01)88606-3