2-[2-(4,4-diethoxybutyl)-N-nosylamino]but-3-enyl-N-nosyl-2,5-dihydropyrrole

Base Information

Chemical Name:2-[2-(4,4-diethoxybutyl)-N-nosylamino]but-3-enyl-N-nosyl-2,5-dihydropyrrole
CAS No.:309248-57-5
Molecular Formula:C₂₈H₃₆N₄O₁₀S₂
Molecular Weight:652.747
Hs Code.:

Synonyms:2-[2-(4,4-diethoxybutyl)-N-nosylamino]but-3-enyl-N-nosyl-2,5-dihydropyrrole

Suppliers and Price of 2-[2-(4,4-diethoxybutyl)-N-nosylamino]but-3-enyl-N-nosyl-2,5-dihydropyrrole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[2-(4,4-diethoxybutyl)-N-nosylamino]but-3-enyl-N-nosyl-2,5-dihydropyrrole

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-[2-(4,4-diethoxybutyl)-N-nosylamino]but-3-enyl-N-nosyl-2,5-dihydropyrrole

There total 1 articles about 2-[2-(4,4-diethoxybutyl)-N-nosylamino]but-3-enyl-N-nosyl-2,5-dihydropyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 309248-40-6
(1S,4R)-N'-(4,4-diethoxybutyl)-N,N'-dinosyl-N-prop-2-enylcyclopent-4-ene-1,3-diamine

: 309248-57-5
2-[2-(4,4-diethoxybutyl)-N-nosylamino]but-3-enyl-N-nosyl-2,5-dihydropyrrole

Guidance literature:: With Grubbs catalyst first generation; ethene; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/ja001688i

Reference yield:

: 309248-57-5
2-[2-(4,4-diethoxybutyl)-N-nosylamino]but-3-enyl-N-nosyl-2,5-dihydropyrrole

: 309248-76-8
(3R,4S)-3-[N-benzyloxycarbonyl-(4,4-diethoxybutyl)amino]-4-(N-benzyloxycarbonyl-2,5-dihydropyrrol-2-yl)butyraldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃; thiophenol / dimethylformamide / 0.5 h / 70 °C

2: 620 mg / dimethylformamide / 0.17 h / 20 °C

3: 72 percent / oxygen; PdCl₂; CuCl / dimethylformamide; H₂O / 6 h

With oxygen; potassium carbonate; thiophenol; copper(l) chloride; palladium dichloride; In water; N,N-dimethyl-formamide;
DOI:10.1021/ja001688i

Reference yield:

: 309248-57-5
2-[2-(4,4-diethoxybutyl)-N-nosylamino]but-3-enyl-N-nosyl-2,5-dihydropyrrole

: 309248-74-6
(2S,7R)-N-benzyloxycarbonyl-2-[2-N-benzyloxycarbonyl-(4,4-diethoxybutyl)amino]-but-3-enyl-2,5-dihydropyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃; thiophenol / dimethylformamide / 0.5 h / 70 °C

2: 620 mg / dimethylformamide / 0.17 h / 20 °C

With potassium carbonate; thiophenol; In N,N-dimethyl-formamide;
DOI:10.1021/ja001688i