2-Bromo-4-methoxy-1-(2-propen-1-yloxy)benzene

Base Information

Chemical Name:2-Bromo-4-methoxy-1-(2-propen-1-yloxy)benzene
CAS No.:68223-99-4
Molecular Formula:C₁₀H₁₁BrO₂
Molecular Weight:243.1
Hs Code.:
DSSTox Substance ID:DTXSID101252661

Synonyms:2-Bromo-4-methoxy-1-(2-propen-1-yloxy)benzene;DTXSID101252661;68223-99-4

Suppliers and Price of 2-Bromo-4-methoxy-1-(2-propen-1-yloxy)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Bromo-4-methoxy-1-(2-propen-1-yloxy)benzene

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:241.99424
Heavy Atom Count:13
Complexity:161

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC(=C(C=C1)OCC=C)Br

Technology Process of 2-Bromo-4-methoxy-1-(2-propen-1-yloxy)benzene

There total 3 articles about 2-Bromo-4-methoxy-1-(2-propen-1-yloxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 17332-11-5
2-bromo-4-methoxyphenol

: 106-95-6
allyl bromide

: 68223-99-4
1-allyloxy-2-bromo-4-methoxybenzene

Guidance literature:: With tetrabutyl ammonium fluoride; potassium carbonate; In acetone; at 55 ℃; for 12h;

Reference yield:

: 150-76-5
4-methoxy-phenol

: 68223-99-4
1-allyloxy-2-bromo-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Br₂ / methanol / 0 - 20 °C

2: 94 percent / K₂CO₃ / acetone / Heating

With bromine; potassium carbonate; In methanol; acetone;
DOI:10.1021/jm060656o

Reference yield:

: 150-76-5
4-methoxy-phenol

: 68223-99-4
1-allyloxy-2-bromo-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Br₂ / CHCl₃ / 0.25 h / 25 °C

2: 80 percent / K₂CO₃ / acetone / 24 h / Heating

With bromine; potassium carbonate; In chloroform; acetone; 1: Bromination / 2: Alkylation;