C₃₉H₆₂N₄O₁₅S

Base Information

Chemical Name:C₃₉H₆₂N₄O₁₅S
CAS No.:1446003-98-0
Molecular Formula:C₃₉H₆₂N₄O₁₅S
Molecular Weight:859.005
Hs Code.:

C<sub>39</sub>H<sub>62</sub>N<sub>4</sub>O<sub>15</sub>S

Synonyms:C₃₉H₆₂N₄O₁₅S

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Chemical Property of C₃₉H₆₂N₄O₁₅S

Chemical Property:

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Technology Process of C₃₉H₆₂N₄O₁₅S

There total 21 articles about C₃₉H₆₂N₄O₁₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14542-16-6
4-methyl-1,3-thiazole-2-carboxylic acid

: 1374760-32-3
C₃₄H₅₉N₃O₁₄

: 1446003-98-0
C₃₉H₆₂N₄O₁₅S

Guidance literature:: 4-methyl-1,3-thiazole-2-carboxylic acid; With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 0.0333333h;

C₃₄H₅₉N₃O₁₄; In N,N-dimethyl-formamide; at 20 ℃; for 1h;

Reference yield:

: 127943-95-7
methyl (1R,3R)-3-(tert-butyldimethylsilyloxy)cyclohex-4-ene-1-carboxylate

: 1446003-98-0
C₃₉H₆₂N₄O₁₅S

Guidance literature:: Multi-step reaction with 12 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 0.5 h / -20 °C / Inert atmosphere

3.1: bromine / dichloromethane / 0.67 h / Cooling with ice

3.2: 17 h / 20 °C / Inert atmosphere; Molecular sieve

3.3: 15 h / 20 °C

4.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

4.2: 2 h / 0 °C / Molecular sieve

5.1: methanol; sodium methylate / 2 h

6.1: triethylamine / acetonitrile / 1.33 h / 0 °C

7.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

7.2: 20 °C

8.1: tri-n-butyl-tin hydride / dichloromethane / 1 h / 20 °C

9.1: palladium 10% on activated carbon; hydrogen; acetic acid / water; 1,4-dioxane / 5 h / 20 °C / 1034.32 Torr

10.1: methanol; sodium methylate / 4 h

11.1: 8 h / 80 °C

12.1: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.03 h / 20 °C

12.2: 1 h / 20 °C

With methanol; n-butyllithium; palladium 10% on activated carbon; hydrogen; bromine; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; HATU; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1374760-24-3
C₁₈H₂₃Cl₃N₂O₁₀

: 1446003-98-0
C₃₉H₆₂N₄O₁₅S

Guidance literature:: Multi-step reaction with 9 steps

1.1: dichloromethane / 0.5 h / 20 °C / Molecular sieve

1.2: 2 h / 0 °C / Molecular sieve

2.1: methanol; sodium methylate / 2 h

3.1: triethylamine / acetonitrile / 1.33 h / 0 °C

4.1: di(n-butyl)tin oxide / methanol / 2 h / Reflux

4.2: 20 °C

5.1: tri-n-butyl-tin hydride / dichloromethane / 1 h / 20 °C

6.1: palladium 10% on activated carbon; hydrogen; acetic acid / water; 1,4-dioxane / 5 h / 20 °C / 1034.32 Torr

7.1: methanol; sodium methylate / 4 h

8.1: 8 h / 80 °C

9.1: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.03 h / 20 °C

9.2: 1 h / 20 °C

With methanol; palladium 10% on activated carbon; hydrogen; tri-n-butyl-tin hydride; sodium methylate; di(n-butyl)tin oxide; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; In 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;