(E)-6-bromo-β-nitro-2-isopropoxy-3,4-dimethoxystyrene

Base Information

Chemical Name:(E)-6-bromo-β-nitro-2-isopropoxy-3,4-dimethoxystyrene
CAS No.:917497-34-8
Molecular Formula:C₁₃H₁₆BrNO₅
Molecular Weight:346.178
Hs Code.:

Synonyms:(E)-6-bromo-β-nitro-2-isopropoxy-3,4-dimethoxystyrene

Suppliers and Price of (E)-6-bromo-β-nitro-2-isopropoxy-3,4-dimethoxystyrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-6-bromo-β-nitro-2-isopropoxy-3,4-dimethoxystyrene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-6-bromo-β-nitro-2-isopropoxy-3,4-dimethoxystyrene

There total 5 articles about (E)-6-bromo-β-nitro-2-isopropoxy-3,4-dimethoxystyrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 917497-33-7
6-bromo-2-isopropoxy-3,4-dimethoxybenzaldehyde

: 75-52-5
nitromethane

: 917497-34-8
(E)-6-bromo-β-nitro-2-isopropoxy-3,4-dimethoxystyrene

Guidance literature:: With ammonium acetate; at 100 ℃; for 0.75h;
DOI:10.1055/s-2006-950191

Reference yield:

: 917497-32-6
6-bromo-2-hydroxy-3,4-dimethoxybenzaldehyde

: 917497-34-8
(E)-6-bromo-β-nitro-2-isopropoxy-3,4-dimethoxystyrene

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / K₂CO₃ / dimethylformamide / 20 °C

2: 100 percent / NH₄OAc / 0.75 h / 100 °C

With ammonium acetate; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1055/s-2006-950191

Reference yield:

: C₉H₉BrO₄

: 917497-34-8
(E)-6-bromo-β-nitro-2-isopropoxy-3,4-dimethoxystyrene

Guidance literature:: Multi-step reaction with 4 steps

1: 5.91 g / aq. KOH / diethyl ether

2: 85 percent / TiCl₄ / CH₂Cl₂ / 4 h / 20 °C

3: 78 percent / K₂CO₃ / dimethylformamide / 20 °C

4: 100 percent / NH₄OAc / 0.75 h / 100 °C

With potassium hydroxide; ammonium acetate; titanium tetrachloride; potassium carbonate; In diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-2006-950191