cis-1-(tert-Butyldimethylsilyloxymethyl)-4-(2-tridecenyloxymethyl)benzene

Base Information

Chemical Name:cis-1-(tert-Butyldimethylsilyloxymethyl)-4-(2-tridecenyloxymethyl)benzene
CAS No.:152124-01-1
Molecular Formula:C₂₇H₄₈O₂Si
Molecular Weight:432.762
Hs Code.:

Synonyms:cis-1-(tert-Butyldimethylsilyloxymethyl)-4-(2-tridecenyloxymethyl)benzene

Suppliers and Price of cis-1-(tert-Butyldimethylsilyloxymethyl)-4-(2-tridecenyloxymethyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of cis-1-(tert-Butyldimethylsilyloxymethyl)-4-(2-tridecenyloxymethyl)benzene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of cis-1-(tert-Butyldimethylsilyloxymethyl)-4-(2-tridecenyloxymethyl)benzene

There total 9 articles about cis-1-(tert-Butyldimethylsilyloxymethyl)-4-(2-tridecenyloxymethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74962-99-5,68480-25-1
(Z)-tridec-2-en-1-ols

: 150864-11-2
tert-butyl((4-(iodomethyl)benzyl)oxy)dimethylsilane

: 152124-01-1
cis-1-(tert-Butyldimethylsilyloxymethyl)-4-(2-tridecenyloxymethyl)benzene

Guidance literature:: With NaH; In tetrahydrofuran;

Reference yield:

: 2050-77-3
Iododecane

: 152124-01-1
cis-1-(tert-Butyldimethylsilyloxymethyl)-4-(2-tridecenyloxymethyl)benzene

Guidance literature:: Multi-step reaction with 4 steps

1: n-BuLi, hexamethylphosphoramide / tetrahydrofuran / 1 h / 0 °C

2: p-TsOH / methanol / 25 °C

3: LiAlH₄ / diethyl ether / 24 h / Heating

4: 1.) NaH / 1.) THF, from 0 deg C to RT, 35 min, 2.) THF, 25 deg C, 12 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium aluminium tetrahydride; n-butyllithium; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; diethyl ether;
DOI:10.1021/jm9606047

Reference yield:

: 51887-25-3
tridec-2-yn-1-ol

: 152124-01-1
cis-1-(tert-Butyldimethylsilyloxymethyl)-4-(2-tridecenyloxymethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether / 24 h / Heating

2: 1.) NaH / 1.) THF, from 0 deg C to RT, 35 min, 2.) THF, 25 deg C, 12 h

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether;
DOI:10.1021/jm9606047