7-tert-butoxycarbonylamino-1,4-diphenyl-5,7,8,9-tetrahydro-benzocyclohepten-6-one

Base Information

Chemical Name:7-tert-butoxycarbonylamino-1,4-diphenyl-5,7,8,9-tetrahydro-benzocyclohepten-6-one
CAS No.:1338797-37-7
Molecular Formula:C₂₈H₂₉NO₃
Molecular Weight:427.543
Hs Code.:

Synonyms:7-tert-butoxycarbonylamino-1,4-diphenyl-5,7,8,9-tetrahydro-benzocyclohepten-6-one

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Chemical Property of 7-tert-butoxycarbonylamino-1,4-diphenyl-5,7,8,9-tetrahydro-benzocyclohepten-6-one

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Technology Process of 7-tert-butoxycarbonylamino-1,4-diphenyl-5,7,8,9-tetrahydro-benzocyclohepten-6-one

There total 14 articles about 7-tert-butoxycarbonylamino-1,4-diphenyl-5,7,8,9-tetrahydro-benzocyclohepten-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1338797-31-1
4-bromo-7-(tert-butoxycarbonylamino)-1-phenyl-5,7,8,9-tetrahydrobenzocyclohepten-6-one

: 98-80-6
phenylboronic acid

: 1338797-37-7
7-tert-butoxycarbonylamino-1,4-diphenyl-5,7,8,9-tetrahydro-benzocyclohepten-6-one

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; at 85 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.bmc.2011.06.089

Reference yield: 79.0%

: 1338797-33-3
1,4-dibromo-7-(tert-butoxycarbonylamino)-5,7,8,9-tetrahydrobenzocyclohepten-6-one

: 98-80-6
phenylboronic acid

: 1338797-37-7
7-tert-butoxycarbonylamino-1,4-diphenyl-5,7,8,9-tetrahydro-benzocyclohepten-6-one

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; at 125 ℃; for 0.416667h; under 2250.23 Torr; Microwave irradiation; Inert atmosphere;
DOI:10.1016/j.bmc.2011.06.089

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₂₃H₂₃NO

: 1338797-37-7
7-tert-butoxycarbonylamino-1,4-diphenyl-5,7,8,9-tetrahydro-benzocyclohepten-6-one

Guidance literature:: di-tert-butyl dicarbonate; C₂₃H₂₃NO; With sodium carbonate; In methanol; at 25 ℃;

With Dess-Martin periodane; In dichloromethane; at 25 ℃; for 2h;
DOI:10.3390/molecules23102607