diethyl (Z)-2-phenyl-1-hydroxyimino-1,2,3,4-tetrahydro-3,3-naphthalenedicarboxylate

Base Information

Chemical Name:diethyl (Z)-2-phenyl-1-hydroxyimino-1,2,3,4-tetrahydro-3,3-naphthalenedicarboxylate
CAS No.:104958-34-1
Molecular Formula:C₂₂H₂₃NO₅
Molecular Weight:381.428
Hs Code.:

Synonyms:diethyl (Z)-2-phenyl-1-hydroxyimino-1,2,3,4-tetrahydro-3,3-naphthalenedicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl (Z)-2-phenyl-1-hydroxyimino-1,2,3,4-tetrahydro-3,3-naphthalenedicarboxylate

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Technology Process of diethyl (Z)-2-phenyl-1-hydroxyimino-1,2,3,4-tetrahydro-3,3-naphthalenedicarboxylate

There total 5 articles about diethyl (Z)-2-phenyl-1-hydroxyimino-1,2,3,4-tetrahydro-3,3-naphthalenedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 104958-17-0
diethyl 2-phenyl-1,2,3,4-tetrahydronapthalene-1-one-3,3-dicarboxylate

: 104958-34-1
diethyl (Z)-2-phenyl-1-hydroxyimino-1,2,3,4-tetrahydro-3,3-naphthalenedicarboxylate

Guidance literature:: With hydroxylamine hydrochloride; In pyridine; for 50h; Heating;

Reference yield:

: 104958-18-1
triethyl 1,3-diphenylpropane-1,2,2-tricarboxylate

: 104958-34-1
diethyl (Z)-2-phenyl-1-hydroxyimino-1,2,3,4-tetrahydro-3,3-naphthalenedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / conc. sulfuric acid / 336 h / 20 °C

2: 45 percent / hydroxylamine hydrochloride / pyridine / 50 h / Heating

With sulfuric acid; hydroxylamine hydrochloride; In pyridine;

Reference yield:

: 2882-19-1,2216-90-2
ethyl 2-phenyl-2-bromoacetate

: 104958-34-1
diethyl (Z)-2-phenyl-1-hydroxyimino-1,2,3,4-tetrahydro-3,3-naphthalenedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 78 percent / sodium ethoxide / ethanol / 20 h / Heating

2: 45 percent / conc. sulfuric acid / 336 h / 20 °C

3: 45 percent / hydroxylamine hydrochloride / pyridine / 50 h / Heating

With sulfuric acid; hydroxylamine hydrochloride; sodium ethanolate; In pyridine; ethanol;