C₁₅H₁₈N₅O₄F₃

Base Information

Chemical Name:C₁₅H₁₈N₅O₄F₃
CAS No.:943601-28-3
Molecular Formula:C₁₅H₁₈F₃N₅O₄
Molecular Weight:389.334
Hs Code.:

C<sub>15</sub>H<sub>18</sub>N<sub>5</sub>O<sub>4</sub>F<sub>3</sub>

Synonyms:C₁₅H₁₈N₅O₄F₃

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Chemical Property of C₁₅H₁₈N₅O₄F₃

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Technology Process of C₁₅H₁₈N₅O₄F₃

There total 6 articles about C₁₅H₁₈N₅O₄F₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 943601-27-2
C₂₀H₂₆N₅O₅F₃

: 943601-28-3
C₁₅H₁₈N₅O₄F₃

Guidance literature:: With (+)-10-camphorsulfonic acid; In methanol; at 20 ℃; for 0.75h;
DOI:10.1021/ol070376i

Reference yield:

: 943601-25-0
C₂₀H₂₅N₂O₆F₃

: 943601-28-3
C₁₅H₁₈N₅O₄F₃

Guidance literature:: Multi-step reaction with 4 steps

1: 735 mg / sodium borohydride / methanol / 0.67 h / 0 °C

2: triethylamine / CH₂Cl₂ / 0.17 h / 20 °C

3: 645 mg / sodium azide; tetra-n-butylammonium iodide / dimethylformamide / 1 h / 60 °C

4: 91 percent / (+)-camphorsulfonic acid / methanol / 0.75 h / 20 °C

With sodium tetrahydroborate; sodium azide; tetra-(n-butyl)ammonium iodide; (+)-10-camphorsulfonic acid; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol070376i

Reference yield:

: 943601-26-1
C₂₀H₂₇N₂O₆F₃

: 943601-28-3
C₁₅H₁₈N₅O₄F₃

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / CH₂Cl₂ / 0.17 h / 20 °C

2: 645 mg / sodium azide; tetra-n-butylammonium iodide / dimethylformamide / 1 h / 60 °C

3: 91 percent / (+)-camphorsulfonic acid / methanol / 0.75 h / 20 °C

With sodium azide; tetra-(n-butyl)ammonium iodide; (+)-10-camphorsulfonic acid; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol070376i