(E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-methylethenyl>benzoyl chloride

Base Information

Chemical Name:(E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-methylethenyl>benzoyl chloride
CAS No.:78315-04-5
Molecular Formula:C₂₄H₂₇ClO
Molecular Weight:366.931
Hs Code.:

Synonyms:(E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-methylethenyl>benzoyl chloride

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Chemical Property of (E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-methylethenyl>benzoyl chloride

Chemical Property:

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Technology Process of (E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-methylethenyl>benzoyl chloride

There total 7 articles about (E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-methylethenyl>benzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 71441-28-6,110917-84-5
TTNPB

: 78315-04-5
(E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-methylethenyl>benzoyl chloride

Guidance literature:: With pyridine; thionyl chloride; N,N-dimethyl-formamide; In diethyl ether;

Reference yield:

: 71441-09-3
AGN 190316

: 78315-04-5
(E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-methylethenyl>benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / potassium hydroxide / H₂O; ethanol / 3 h / 50 °C

2: thionyl chloride, pyridine / N,N-dimethylformamide / diethyl ether

With pyridine; potassium hydroxide; thionyl chloride; N,N-dimethyl-formamide; In diethyl ether; ethanol; water;

Reference yield:

: 17610-21-8
1-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphth-2-yl)ethanone

: 78315-04-5
(E)-4-<2-(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphthyl)-2-methylethenyl>benzoyl chloride

Guidance literature:: Multi-step reaction with 6 steps

1: sodium borohydride / methanol / 1.5 h / 0 °C

2: phosphorus tribromide / pyridine / diethyl ether; hexane / 2.5 h / 0 - 5 °C

3: diethyl ether; xylene / 48 h / 100 °C

4: 69.3 percent / butylene oxide / 12 h / 65 °C

5: 86 percent / potassium hydroxide / H₂O; ethanol / 3 h / 50 °C

6: thionyl chloride, pyridine / N,N-dimethylformamide / diethyl ether

With tetrahydrofuran; pyridine; potassium hydroxide; sodium tetrahydroborate; thionyl chloride; phosphorus tribromide; pyridine; N,N-dimethyl-formamide; In methanol; diethyl ether; ethanol; hexane; water; xylene;