(S)-4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoyl chloride

Base Information

Chemical Name:(S)-4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoyl chloride
CAS No.:1456507-72-4
Molecular Formula:C₁₉H₁₈ClNO₃
Molecular Weight:343.81
Hs Code.:

Synonyms:(S)-4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoyl chloride

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Chemical Property of (S)-4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoyl chloride

Chemical Property:

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Technology Process of (S)-4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoyl chloride

There total 4 articles about (S)-4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1456507-71-3
(S)-4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoic acid

: 1456507-72-4
(S)-4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoyl chloride

Guidance literature:: With thionyl chloride; In dichloromethane; at 40 ℃; for 1h;

Reference yield:

: 99548-55-7
4-bromo-2-methyl-benzoic acid methyl ester

: 1456507-72-4
(S)-4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1: potassium phosphate; N,N`-dimethylethylenediamine; copper(l) iodide / 1,4-dioxane / 1 h / 140 °C / Inert atmosphere; Microwave irradiation; Sealed tube

2: water; lithium hydroxide / methanol; tetrahydrofuran / 16 h / 50 °C

3: thionyl chloride / dichloromethane / 1 h / 40 °C

With potassium phosphate; copper(l) iodide; thionyl chloride; water; lithium hydroxide; N,N`-dimethylethylenediamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane;

Reference yield:

: 1456507-70-2
(S)-methyl 4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoate

: 1456507-72-4
(S)-4-(5,5-dimethyl-2-oxo-4-phenyloxazolidin-3-yl)-2-methylbenzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: water; lithium hydroxide / methanol; tetrahydrofuran / 16 h / 50 °C

2: thionyl chloride / dichloromethane / 1 h / 40 °C

With thionyl chloride; water; lithium hydroxide; In tetrahydrofuran; methanol; dichloromethane;