BENZOIC ACID,4-BROMO-2-METHYL-,METHYL ESTER

Base Information

• Chemical Name: BENZOIC ACID,4-BROMO-2-METHYL-,METHYL ESTER
• CAS No.: 99548-55-7
• Molecular Formula: C9H9BrO2
• Molecular Weight: 229.073
• Hs Code.: 2916399090
• Mol file: 99548-55-7.mol

Synonyms:o-Toluic acid, 4-bromo-, methyl ester (6CI);4-Bromo-2-methylbenzoic acid methyl ester;Methyl 4-bromo-o-toluate;

Chemical Property of BENZOIC ACID,4-BROMO-2-METHYL-,METHYL ESTER

Chemical Property:

• Vapor Pressure: 0.006mmHg at 25°C
• Melting Point: 9 °C
• Refractive Index: 1.545
• Boiling Point: 273.627 °C at 760 mmHg
• Flash Point: 119.286 °C
• PSA: 26.30000
• Density: 1.434 g/cm³
• LogP: 2.54410
• Storage Temp.: 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

Methyl4-Bromo-2-methylbenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of BENZOIC ACID,4-BROMO-2-METHYL-,METHYL ESTER

There total 8 articles about BENZOIC ACID,4-BROMO-2-METHYL-,METHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-bromo-2-methylbenzoic acid (68837-59-2) + diazomethyl-trimethyl-silane (18107-18-1) → 4-bromo-2-methyl-benzoic acid methyl ester (99548-55-7)

Guidance literature:

In dichloromethane;

DOI:10.1016/j.bmcl.2004.12.036

Reference yield: 100.0%

4-bromo-2-methylbenzoic acid (68837-59-2) + methyl iodide (74-88-4) → 4-bromo-2-methyl-benzoic acid methyl ester (99548-55-7)

Guidance literature:

With sodium hydrogencarbonate; In N,N-dimethyl-formamide; at 80 ℃;

Reference yield: 100.0%

4-bromo-2-methylbenzoic acid (68837-59-2) → 4-bromo-2-methyl-benzoic acid methyl ester (99548-55-7)

Guidance literature:

With hydrogenchloride; In methanol;

upstream raw materials:

methanol

4-bromo-2-methylbenzoic acid

diazomethyl-trimethyl-silane

methyl iodide

Downstream raw materials:

4-bromo-2-methylbenzohydrazide

4-Cyclohexyl-2-methyl-benzoic acid methyl ester

methyl 4-cyclobutyl-2-methylbenzoate

2-Methyl-4-propyl-benzoic acid methyl ester

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