C₄₅H₄₄N₄O₁₂P₂S₅

Base Information

Chemical Name:C₄₅H₄₄N₄O₁₂P₂S₅
CAS No.:84752-73-8
Molecular Formula:C₄₅H₄₄N₄O₁₂P₂S₅
Molecular Weight:1055.14
Hs Code.:

C<sub>45</sub>H<sub>44</sub>N<sub>4</sub>O<sub>12</sub>P<sub>2</sub>S<sub>5</sub>

Synonyms:C₄₅H₄₄N₄O₁₂P₂S₅

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Chemical Property of C₄₅H₄₄N₄O₁₂P₂S₅

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Technology Process of C₄₅H₄₄N₄O₁₂P₂S₅

There total 7 articles about C₄₅H₄₄N₄O₁₂P₂S₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21090-30-2
3'-O-acetylthymidine

: 84752-73-8
C₄₅H₄₄N₄O₁₂P₂S₅

Guidance literature:: Multi-step reaction with 5 steps

1: 53 percent / TsOH*H₂O, molecular sieves / dioxane / 1 h

2: 96 percent / BuNH₂ / methanol / 3 h / Ambient temperature

3: 87 percent / mesitylene 1,3-disulfonyl chloride / pyridine / 5 h

4: pyridinium phosphinate, TEA / pyridine / 0.25 h / Ambient temperature

5: mesitylene 1,3-disulfonyl chloride, 3-nitro-1,2,4-triazole / pyridine / 0.67 h / Ambient temperature

With molecular sieve; H₂O₂P*C₅H₅N; TEA; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; toluene-4-sulfonic acid; N-butylamine; 3-nitro-1,2,4-triazole; In 1,4-dioxane; pyridine; methanol;
DOI:10.1021/ja00345a062

Reference yield:

: 67941-87-1
cyclohexylammonium S,S-diphenyl phosphorodithioate

: 84752-73-8
C₄₅H₄₄N₄O₁₂P₂S₅

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / mesitylene 1,3-disulfonyl chloride / pyridine / 5 h

2: pyridinium phosphinate, TEA / pyridine / 0.25 h / Ambient temperature

3: mesitylene 1,3-disulfonyl chloride, 3-nitro-1,2,4-triazole / pyridine / 0.67 h / Ambient temperature

With H₂O₂P*C₅H₅N; TEA; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; 3-nitro-1,2,4-triazole; In pyridine;
DOI:10.1021/ja00345a062

Reference yield:

: 84752-63-6
5'-O-(1,3-benzodithiol-2-yl)thymidine

: 84752-73-8
C₄₅H₄₄N₄O₁₂P₂S₅

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / mesitylene 1,3-disulfonyl chloride / pyridine / 5 h

2: pyridinium phosphinate, TEA / pyridine / 0.25 h / Ambient temperature

3: mesitylene 1,3-disulfonyl chloride, 3-nitro-1,2,4-triazole / pyridine / 0.67 h / Ambient temperature

With H₂O₂P*C₅H₅N; TEA; 2,4,6-trimethyl-1,3-benzenedisulfonyl dichloride; 3-nitro-1,2,4-triazole; In pyridine;
DOI:10.1021/ja00345a062