C₁₈H₂₉BrO₃

Base Information

Chemical Name:C₁₈H₂₉BrO₃
CAS No.:1526928-68-6
Molecular Formula:C₁₈H₂₉BrO₃
Molecular Weight:373.33
Hs Code.:

C<sub>18</sub>H<sub>29</sub>BrO<sub>3</sub>

Synonyms:C₁₈H₂₉BrO₃

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Chemical Property of C₁₈H₂₉BrO₃

Chemical Property:

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Technology Process of C₁₈H₂₉BrO₃

There total 1 articles about C₁₈H₂₉BrO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 500-99-2
3,5-dimethoxyphenol

: 4101-68-2
1,10-dibromodecane

: 1526928-68-6
C₁₈H₂₉BrO₃

Guidance literature:: 3,5-dimethoxyphenol; With potassium carbonate; In acetonitrile; at 20 ℃; for 0.5h; Inert atmosphere;

1,10-dibromodecane; In acetonitrile; Inert atmosphere; Reflux;
DOI:10.1039/c3cc48014c

Reference yield:

: 1526928-68-6
C₁₈H₂₉BrO₃

: 1526928-69-7
C₁₈H₃₁NO₃

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / acetone; water / 24 h / Inert atmosphere; Reflux

2: palladium on activated charcoal; hydrogen / methanol; chloroform / 24 h / Reflux

With sodium azide; palladium on activated charcoal; hydrogen; In methanol; chloroform; water; acetone;
DOI:10.1039/c3cc48014c

Reference yield:

: 1526928-68-6
C₁₈H₂₉BrO₃

: 1526928-70-0
C₆₄H₇₉NO₁₄

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / acetone; water / 24 h / Inert atmosphere; Reflux

2: palladium on activated charcoal; hydrogen / methanol; chloroform / 24 h / Reflux

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 24 h / -20 °C

With dmap; sodium azide; palladium on activated charcoal; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In methanol; dichloromethane; chloroform; water; acetone;
DOI:10.1039/c3cc48014c