bis[4-(N-carbazolyl)-2,6-dichlorophenyl](2,4,6-trichlorophenyl)methyl

Base Information

Chemical Name:bis[4-(N-carbazolyl)-2,6-dichlorophenyl](2,4,6-trichlorophenyl)methyl
CAS No.:1018803-11-6
Molecular Formula:C₄₃H₂₂Cl₇N₂
Molecular Weight:814.832
Hs Code.:

Synonyms:bis[4-(N-carbazolyl)-2,6-dichlorophenyl](2,4,6-trichlorophenyl)methyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis[4-(N-carbazolyl)-2,6-dichlorophenyl](2,4,6-trichlorophenyl)methyl

Chemical Property:

Purity/Quality:

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Technology Process of bis[4-(N-carbazolyl)-2,6-dichlorophenyl](2,4,6-trichlorophenyl)methyl

There total 5 articles about bis[4-(N-carbazolyl)-2,6-dichlorophenyl](2,4,6-trichlorophenyl)methyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₃₆N⁽¹⁺⁾*C₄₃H₂₂Cl₇N₂^(1-)

: 1018803-11-6
bis[4-(N-carbazolyl)-2,6-dichlorophenyl](2,4,6-trichlorophenyl)methyl

Guidance literature:: With chloranil; In tetrahydrofuran; water; for 2.5h;
DOI:10.1021/jo702723k

Reference yield:

: 105633-27-0
tris(2,4,6-trichlorophenyl)methane

: 1018803-11-6
bis[4-(N-carbazolyl)-2,6-dichlorophenyl](2,4,6-trichlorophenyl)methyl

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetra(n-butyl)ammonium hydroxide / methanol; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Darkness

1.2: 1 h / Inert atmosphere; Darkness

2.1: caesium carbonate / N,N-dimethyl-formamide / 2.17 h / 160 °C / Inert atmosphere; Darkness

3.1: tetra(n-butyl)ammonium hydroxide / methanol; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Darkness

3.2: 1 h / Inert atmosphere; Darkness

4.1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 160 °C / Inert atmosphere; Darkness

5.1: tetra(n-butyl)ammonium hydroxide / methanol; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Darkness

5.2: 1 h / Inert atmosphere; Darkness

With tetra(n-butyl)ammonium hydroxide; caesium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201500242

Reference yield:

: 109745-46-2
tris(2,4,6‐trichlorophenyl)methyl radical

: 1018803-11-6
bis[4-(N-carbazolyl)-2,6-dichlorophenyl](2,4,6-trichlorophenyl)methyl

Guidance literature:: Multi-step reaction with 4 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 2.17 h / 160 °C / Inert atmosphere; Darkness

2.1: tetra(n-butyl)ammonium hydroxide / methanol; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Darkness

2.2: 1 h / Inert atmosphere; Darkness

3.1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 160 °C / Inert atmosphere; Darkness

4.1: tetra(n-butyl)ammonium hydroxide / methanol; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere; Darkness

4.2: 1 h / Inert atmosphere; Darkness

With tetra(n-butyl)ammonium hydroxide; caesium carbonate; In tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.201500242