1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)perylene-3,4-dicarboxylic anhydride

Base Information

Chemical Name:1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)perylene-3,4-dicarboxylic anhydride
CAS No.:1307916-81-9
Molecular Formula:C₄₆H₄₁NO₅
Molecular Weight:687.835
Hs Code.:

Synonyms:1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)perylene-3,4-dicarboxylic anhydride

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Chemical Property of 1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)perylene-3,4-dicarboxylic anhydride

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Technology Process of 1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)perylene-3,4-dicarboxylic anhydride

There total 4 articles about 1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)perylene-3,4-dicarboxylic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1307916-80-8
1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide

: 1307916-81-9
1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)perylene-3,4-dicarboxylic anhydride

Guidance literature:: 1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)-N-(2,5-di-tert-butylphenyl)perylene-3,4-dicarboximide; With potassium hydroxide; In tert-butyl alcohol; for 3h; Reflux;

With acetic acid; In water; tert-butyl alcohol; at 20 ℃;
DOI:10.1039/c0cc05755j

Reference yield:

: 1,6-bis(4-tert-butylphenoxy)-9-[2-(bromide)ethynyl]-N-(2,5-di-tert-butylphenyl)-3,4-perylenedicarboximide

: 1307916-81-9
1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)perylene-3,4-dicarboxylic anhydride

Guidance literature:: Multi-step reaction with 2 steps

1.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 100 °C

2.1: potassium hydroxide / tert-butyl alcohol / 3 h / Reflux

2.2: 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; potassium hydroxide; sodium t-butanolate; In toluene; tert-butyl alcohol;
DOI:10.1039/c0cc05755j

Reference yield:

: 165261-25-6
N-(2,5-di-tert-butylphenyl)-perylene-3,4-dicarboxylic imide

: 1307916-81-9
1-(N-pyrrolidino)-6,9-di(tert-butoxyphenoxy)perylene-3,4-dicarboxylic anhydride

Guidance literature:: Multi-step reaction with 4 steps

1.1: bromine / chloroform / 19 h / Reflux

2.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 100 °C

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate / toluene / 100 °C

4.1: potassium hydroxide / tert-butyl alcohol / 3 h / Reflux

4.2: 20 °C

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; bromine; potassium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; potassium hydroxide; sodium t-butanolate; In chloroform; N,N-dimethyl-formamide; toluene; tert-butyl alcohol;
DOI:10.1039/c0cc05755j