3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-trifluoromethyluridine

Base Information

Chemical Name:3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-trifluoromethyluridine
CAS No.:182004-61-1
Molecular Formula:C₃₂H₂₂F₆N₂O₉
Molecular Weight:692.525
Hs Code.:

Synonyms:3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-trifluoromethyluridine

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Chemical Property of 3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-trifluoromethyluridine

Chemical Property:

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Technology Process of 3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-trifluoromethyluridine

There total 3 articles about 3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-trifluoromethyluridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 145828-13-3
α-D-1,3,5-tri-O-benzoyl-2-O-[3-(trifluoromethyl)benzoyl]ribofuranose

: 7057-43-4
5-trifluoromethyl-2,4-bis(trimethylsilyloxy)pyrimidine

: 182004-61-1
3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-trifluoromethyluridine

Guidance literature:: With tin(IV) chloride; In acetonitrile;
DOI:10.1021/jo960936j

Reference yield:

: 22224-41-5
1,3,5-tri-O-benzoyl-α-D-ribofuranoside

: 182004-61-1
3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-trifluoromethyluridine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / 2,6-lutidine / CH₂Cl₂ / 2.5 h / 20 °C

2: 97 percent / SnCl₄ / acetonitrile / 20 °C

With 2,6-dimethylpyridine; tin(IV) chloride; In dichloromethane; acetonitrile; 1: Acylation / 2: Substitution;
DOI:10.1021/jo0003652

Reference yield:

: 2251-65-2
3-(Trifluoromethyl)benzoyl chloride

: 182004-61-1
3',5'-di-O-benzoyl-2'-O-[3-(trifluoromethyl)benzoyl]-5-trifluoromethyluridine

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / 2,6-lutidine / CH₂Cl₂ / 2.5 h / 20 °C

2: 97 percent / SnCl₄ / acetonitrile / 20 °C

With 2,6-dimethylpyridine; tin(IV) chloride; In dichloromethane; acetonitrile; 1: Acylation / 2: Substitution;
DOI:10.1021/jo0003652