Technology Process of C24H22ClN3O3
There total 6 articles about C24H22ClN3O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine;
In
dichloromethane;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sulfuric acid; nitric acid / 0.5 h / 0 °C
2: trichlorophosphate / 106 °C
3: iron; acetic acid / 2 h / 40 °C
4: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; N,N-dimethyl-formamide / 0.67 h / 130 °C / Microwaves
5: pyridine / dichloromethane / 1 h
With
pyridine; sulfuric acid; nitric acid; iron; potassium carbonate; acetic acid; trichlorophosphate;
tetrakis(triphenylphosphine) palladium(0);
In
dichloromethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: trichlorophosphate / 106 °C
2: iron; acetic acid / 2 h / 40 °C
3: potassium carbonate / tetrakis(triphenylphosphine) palladium(0) / water; N,N-dimethyl-formamide / 0.67 h / 130 °C / Microwaves
4: pyridine / dichloromethane / 1 h
With
pyridine; iron; potassium carbonate; acetic acid; trichlorophosphate;
tetrakis(triphenylphosphine) palladium(0);
In
dichloromethane; water; N,N-dimethyl-formamide;