N⁽³⁾,N⁽⁵⁾-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide

Base Information

• Chemical Name: N⁽³⁾,N⁽⁵⁾-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide
• CAS No.: 912901-37-2
• Molecular Formula: C₂₃H₂₀N₄O₃S
• Molecular Weight: 432.503

Synonyms:N⁽³⁾,N⁽⁵⁾-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide

Chemical Property of N⁽³⁾,N⁽⁵⁾-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide

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Technology Process of N⁽³⁾,N⁽⁵⁾-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide

There total 1 articles about N⁽³⁾,N⁽⁵⁾-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

3-amino-3-thioxo-N-phenylpropanamide (59749-96-1) + (Z)-2-Cyano-3-furan-2-yl-N-phenyl-acrylamide (5428-38-6) → N(3),N(5)-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide (912901-37-2)

Guidance literature:

3-amino-N-phenyl-3-thioxopropanamide; With sodium ethanolate; In ethanol; at 20 ℃; for 0.166667h;

(Z)-2-Cyano-3-furan-2-yl-N-phenyl-acrylamide; In ethanol; at 20 ℃; for 2h; chemoselective reaction;

DOI:10.1007/s10593-008-0114-5

Reference yield: 70.0%

N(3),N(5)-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide (912901-37-2) + methyl iodide (74-88-4) → N(3),N(5)-diphenyl-6-amino-4-(2-furyl)-2-methylthio-3,4-dihydropyridine-3,5-dicarboxamide (1146770-67-3)

Guidance literature:

N⁽³⁾,N⁽⁵⁾-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide; With sodium ethanolate; In ethanol; at 20 ℃; for 0.166667h;

methyl iodide; In ethanol; at 20 ℃; for 48h;

DOI:10.1007/s10593-008-0114-5

Reference yield: 58.0%

N(3),N(5)-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide (912901-37-2) + benzyl chloride (100-44-7) → N(3),N(5)-diphenyl-6-benzylthio-4-(2-furyl)-2-oxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide (1146770-73-1)

Guidance literature:

N⁽³⁾,N⁽⁵⁾-diphenyl-6-amino-4-(2-furyl)-2-thioxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide; With potassium hydroxide; water; In ethanol; at 50 ℃;

benzyl chloride; In ethanol; water; for 48h;

DOI:10.1007/s10593-008-0114-5

upstream raw materials:

3-amino-3-thioxo-N-phenylpropanamide

(Z)-2-Cyano-3-furan-2-yl-N-phenyl-acrylamide

Downstream raw materials:

N⁽³⁾,N⁽⁵⁾-diphenyl-6-benzylthio-4-(2-furyl)-2-oxo-1,2,3,4-tetrahydropyridine-3,5-dicarboxamide

N⁽³⁾,N⁽⁵⁾-diphenyl-6-amino-4-(2-furyl)-2-methylthio-3,4-dihydropyridine-3,5-dicarboxamide

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