(2S,3R)-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-5-methyl-2-(4-nitro-benzenesulfonylamino)-hex-4-enoic acid ethyl ester

Base Information

Chemical Name:(2S,3R)-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-5-methyl-2-(4-nitro-benzenesulfonylamino)-hex-4-enoic acid ethyl ester
CAS No.:1243256-58-7
Molecular Formula:C₄₇H₅₁N₃O₉S₂Si
Molecular Weight:894.154
Hs Code.:

(2S,3R)-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-5-methyl-2-(4-nitro-benzenesulfonylamino)-hex-4-enoic acid ethyl ester

Synonyms:(2S,3R)-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-5-methyl-2-(4-nitro-benzenesulfonylamino)-hex-4-enoic acid ethyl ester

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Chemical Property of (2S,3R)-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-5-methyl-2-(4-nitro-benzenesulfonylamino)-hex-4-enoic acid ethyl ester

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Technology Process of (2S,3R)-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-5-methyl-2-(4-nitro-benzenesulfonylamino)-hex-4-enoic acid ethyl ester

There total 1 articles about (2S,3R)-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-5-methyl-2-(4-nitro-benzenesulfonylamino)-hex-4-enoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1243256-66-7
C₄₁H₄₈N₂O₅SSi

: 98-74-8
4-Nitrobenzenesulfonyl chloride

: 1243256-58-7
(2S,3R)-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-5-methyl-2-(4-nitro-benzenesulfonylamino)-hex-4-enoic acid ethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In acetonitrile; at 0 ℃; for 0.5h;
DOI:10.1016/j.tet.2010.06.092

Reference yield: 27.0%

: 1243256-58-7
(2S,3R)-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-5-methyl-2-(4-nitro-benzenesulfonylamino)-hex-4-enoic acid ethyl ester

: 1305343-12-7
C₃₁H₃₁N₃O₈S₂

: 1305343-28-5
C₃₁H₃₁N₃O₈S₂

: 1305343-13-8
C₂₉H₂₇N₃O₈S₂

: 1305343-14-9
C₃₁H₃₁N₃O₈S₂

Guidance literature:: (2S,3R)-3-[4-(tert-butyl-diphenyl-silanyloxymethyl)-1-(toluene-4-sulfonyl)-1H-indol-3-yl]-5-methyl-2-(4-nitro-benzenesulfonylamino)-hex-4-enoic acid ethyl ester; With trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

With sodium hydrogencarbonate; In dichloromethane;
DOI:10.1016/j.tet.2011.03.002